103-74-2

2-羥乙基吡啶(103-74-2)質(zhì)譜(MS)

產(chǎn)品名稱:2-羥乙基吡啶

CAS:103-74-2

分子式:C7H9NO

分子量: 123.15

InChI:InChI=1S/C7H9NO/c9-6-4-7-3-1-2-5-8-7/h1-3,5,9H,4,6H2

InChIKey: BXGYBSJAZFGIPX-UHFFFAOYSA-N

Smiles:C1(CCO)=NC=CC=C1

Mass

MS-NW-3756          
2-pyridineethanol
C7H9NO              (Mass of molecular ion:    123)

   Source Temperature: 200 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       1.0
      18.0       2.4
      26.0       2.8
      27.0       5.5
      28.0       4.0
      29.0       2.4
      31.0       9.2
      37.0       1.8
      38.0       3.5
      39.0      17.1
      40.0       4.1
      41.0       3.2
      42.0       1.5
      50.0       5.6
      51.0      12.0
      52.0      14.1
      53.0       5.0
      54.0       1.6
      62.0       1.2
      63.0       3.6
      64.0       2.7
      65.0      18.9
      66.0      18.9
      67.0       5.2
      77.0       2.1
      78.0      11.7
      79.0      43.1
      80.0       9.5
      92.0      14.1
      93.0     100.0
      94.0      13.0
     104.0       7.1
     105.0      19.0
     106.0      89.8
     107.0       7.2
     108.0       1.1
     122.0      25.0
     123.0      14.1
     124.0       1.3

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₇ H₉ N O	0.04 ml : 0.5 ml CDCl₃
2-pyridineethanol

    Assign.     Shift(ppm)

      A             8.449
      B             7.589
      C             7.16
      D             7.14
      E             4.59
      F             3.994
      G             3.010

     Hz     ppm     Int.

    760.75   8.495    130
    759.63   8.482    164
    758.94   8.475    178
    758.00   8.464    158
    756.00   8.442    142
    754.88   8.429    167
    753.94   8.419    178
    753.06   8.409    169
    689.63   7.701    122
    687.75   7.680    123
    682.38   7.620    168
    681.56   7.611    193
    680.31   7.597    215
    679.88   7.592    217
    674.38   7.530    258
    672.50   7.509    247
    647.19   7.227     92
    645.88   7.212    355
    645.38   7.207    265
    644.69   7.199    316
    644.06   7.192    321
    642.75   7.177    108
    639.31   7.139    278
    637.88   7.123    313
    637.38   7.117    272
    636.88   7.112    288
    635.56   7.097    122
    631.94   7.057    130
    631.50   7.052     92
    631.06   7.047     84
    630.69   7.043    111
    411.00   4.590    354
    364.13   4.066    444
    358.19   4.000   1000
    353.50   3.948     66
    352.25   3.934    620
    275.13   3.073    392
    269.19   3.006    615
    263.38   2.941    299

in CDCl3