2,6-Dichlorophenylhydrazine hydrochloride(50709-36-9) Raman

Product Name2,6-Dichlorophenylhydrazine hydrochloride

CAS 50709-36-9

Molecular FormulaC6H7Cl3N2

Molecular Weight213.49

InChIInChI=1S/C6H6Cl2N2.ClH/c7-4-2-1-3-5(8)6(4)10-9;/h1-3,10H,9H2;1H

InChIKey CQNIYLLTIOPFCJ-UHFFFAOYSA-N

SmilesC1(NN)=C(Cl)C=CC=C1Cl.Cl

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2,6-Dichlorophenylhydrazine hydrochloride(50709-36-9) Raman
Mass

MS-NW-6484          
(2,6-dichlorophenyl)hydrazine hydrochloride
C6H6Cl2N2 HCl       (Mass of molecular ion:    176)

   Source Temperature: 110 °C
   Sample Temperature:  90 °C
   Direct, 75 eV

      16.0       1.4
      17.0       1.9
      18.0      10.4
      28.0       4.5
      29.0       4.2
      30.0       1.6
      31.0       4.3
      35.0       5.8
      36.0      59.6
      37.0       4.2
      38.0      19.3
      39.0       2.5
      44.5       1.8
      47.0       1.3
      49.0       2.2
      50.0       6.0
      51.0       7.9
      52.0       7.3
      61.0       3.2
      62.0       5.0
      63.0       7.4
      64.0       2.1
      72.0       1.8
      73.0       7.4
      74.0       7.4
      75.0      16.8
      76.0      11.6
      77.0       7.1
      78.0       4.4
      83.0       1.0
      84.0       2.7
      85.0       2.7
      86.0       1.7
      87.0       1.6
      88.0       3.1
      89.0       1.8
      90.0       3.4
      97.0       2.2
      98.0       2.1
      99.0       3.3
     101.0       1.0
     105.0       1.6
     107.0       1.1
     109.0       2.5
     110.0       2.2
     111.0      14.4
     112.0       3.9
     113.0       5.2
     114.0       3.3
     124.0      11.7
     125.0       7.4
     126.0       5.0
     127.0       2.6
     133.0      27.4
     134.0       1.7
     135.0      18.6
     136.0       1.1
     137.0       3.0
     139.0       1.3
     141.0       6.5
     143.0       2.0
     146.0       8.0
     147.0       1.4
     148.0       5.6
     159.0       4.5
     160.0      59.5
     161.0      24.2
     162.0      39.1
     163.0      14.2
     164.0       7.3
     165.0       2.4
     175.0       1.7
     176.0     100.0
     177.0       8.3
     178.0      64.3
     179.0       5.0
     180.0      11.0

400 MHz in DMSO-d6

2,6-Dichlorophenylhydrazine hydrochloride(50709-36-9) Raman

¹H NMR	399.65 MHz
C₆ H₆ Cl₂ N₂	0.040 g : 0.5 ml DMSO-d₆
(2,6-dichlorophenyl)hydrazine hydrochloride

    Assign.     Shift(ppm)

      A            10.4
      B             7.537
      C             7.292
      D             7.23

     Hz     ppm     Int.

   4147.25  10.378    110
   3016.94   7.549    820
   3013.64   7.541     28
   3012.17   7.538     33
   3008.88   7.529   1000
   2921.87   7.312    303
   2914.18   7.292    375
   2913.45   7.291    312
   2905.75   7.271    234
   2890.55   7.233    102

in DMSO-d6