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CAS No. : | 1025-15-6 | MDL No. : | MFCD00006554 |
Formula : | C12H15N3O3 | Boiling Point : | No data available |
Linear Structure Formula : | C3O3(NCH2CHCH2)3 | InChI Key : | KOMNUTZXSVSERR-UHFFFAOYSA-N |
M.W : | 249.27 | Pubchem ID : | 13931 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | |
Hazard Statements: | H302 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With platinum; In toluene; at 119 - 130℃; for 48h; | 1) taking 0.5 g of hydrosilylation catalyst platinum, diluted with 5 mL of toluene, and then added to a 250 mL three-necked flask;(2) Take 2.49g of 1,3,5-triallyl-1,3,5-triazine-2,4,6(1H,3H,5H)-trione (1,3,5-Triallyl-1,3,5-triazine-2,4,6(1H,3H,5H)-trione, molecular weight MW=249.27g/mol), diluted with 20mL of toluene and added to a three-necked flask;(3) taking 8.75 g of 1,4-Bis (dimethylsilyl)benzene (molecular weight = 194.42), adding 25 mL of toluene and adding to a three-necked flask;(4) setting the oil bath temperature to 130 C, turning on the stirring, turning on the condensed water, and when the temperature in the three-necked flask is 119 C, the reaction mixture starts to reflux;(5) After refluxing for a while, a small amount of the reaction mixture is taken for IR test to determine whether the reaction is complete.(6) After 48 hours, the IR results showed that the carbon-free carbon double bond absorption peak indicates the end of the reaction, and the 1H NMR results showed no vinyl H. At this time, the reaction mixture was transferred to a rotary evaporator to distill off the solvent, and the product cross-linking agent was precipitated. 4 |