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CAS No. : | 96-54-8 | MDL No. : | MFCD00005345 |
Formula : | C5H7N | Boiling Point : | No data available |
Linear Structure Formula : | C4H4N(CH3) | InChI Key : | OXHNLMTVIGZXSG-UHFFFAOYSA-N |
M.W : | 81.12 | Pubchem ID : | 7304 |
Synonyms : |
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Signal Word: | Danger | Class: | 3 |
Precautionary Statements: | P210-P261-P305+P351+P338 | UN#: | 1993 |
Hazard Statements: | H225-H315-H319-H335 | Packing Group: | Ⅱ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
82% | With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 25℃; for 0.5h; | General procedure: The mixture of asodium arylsulfinate (0.2 mmol, 1.0 equiv), a pyrrole/thiophene (0.3 mmol, 1.5equiv) and TMSOTf (0.4 mmol, 2.0 equiv) in (ClCH2)2 (1.0 mL) was stirred at25 C for 0.5 h, then water (5 mL) and dichloromethane (10 mL) were added.The two layers were separated, and the aqueous phase was extracted withdichloromethane (3 × 10 mL). The combined organic extracts were washed bybrine, dried over anhydrous Na2SO4, filtered, and concentrated. The residuewas purified by flash chromatography on silica gel (ethyl acetate : petroleumether = 1:1) to afford the desired sulfoxides 4. |
[ 43036-06-2 ]
3-(1H-Pyrrol-1-yl)propanenitrile
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