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CAS No. : | 94142-97-9 | MDL No. : | MFCD03001669 |
Formula : | C10H14O3 | Boiling Point : | - |
Linear Structure Formula : | C6H4(CH3)2(O)2(C(CH3)OH) | InChI Key : | DIJDAMFZOHSRID-UHFFFAOYSA-N |
M.W : | 182.22 | Pubchem ID : | 566977 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
52% | General procedure: To 2-acetyl-1,3-indandione 8 (1.88 g, 10 mmol) and correspondingderivative of benzaldehyde 1,3,4,7,10 (10 mmol) piperidine(5 mmol) was added. Reaction mixture was refluxed at 110 Cfor 4 h, then it was cooled to 80 C and 8 ml of ethanol was added.Solution was boiled for 30 min, and after cooling, the formedcrystals were filtered off and washed with ethanol. Products wererecrystallized from CH2Cl2 and EtOH mixture. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
77% | With N-ethyl-N,N-diisopropylamine; In ethanol; at 25℃; for 20h; | (3) 70.5 g (0.21 mol) of fmoc-dab-OH was added to the reactor,Then add 705 ml of absolute ethanol and then add 57.4 g (0.32 mol) of DDE-OH.Then, 27.1 g (0.21 mol) of DIEA was used, and then the temperature was raised to 25 C for 20 h.The reaction was followed by TLC, and after completion of the reaction, it was washed twice with ethyl ether petroleum ether mixture.Extraction with citric acid acidified ethyl acetate, washing with citric acid, washing with water, washing with saturated brine, drying and concentrating.And adding petroleum ether crystals to obtain a white solid, which is determined by nuclear magnetic resonance and mass spectrometry.That is, fmoc-dab(DDE)-OH, dried to obtain 80.5 g, and the yield was 77%. |