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Chemical Structure| 937048-76-5 Chemical Structure| 937048-76-5
Chemical Structure| 937048-76-5

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CAS No.: 937048-76-5

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Product Details of [ 937048-76-5 ]

CAS No. :937048-76-5
Formula : C20H30BNO4
M.W : 359.27
SMILES Code : O=C(N1CC2=C(C=CC(B3OC(C)(C)C(C)(C)O3)=C2)CC1)OC(C)(C)C
MDL No. :MFCD11044674
InChI Key :UPDWDCOAUJYOTG-UHFFFAOYSA-N
Pubchem ID :53302321

Safety of [ 937048-76-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis [ 937048-76-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 937048-76-5 ]

[ 937048-76-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 937048-76-5 ]
  • [ 81093-21-2 ]
  • tert-butyl 7-(2,3-dimethylbenzyl)-3,4-dihydroisoquinoline-2(1H)-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
52% With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In water; acetone; at 100℃; for 0.5h;Microwave irradiation; Inert atmosphere; General procedure: The appropriate benzyl bromide (1.5-2.0 eq), intermediate 6 (1.0 eq), Pd(dppf)Cl2 (0.1 eq), andK2CO3 (3.0 eq) were combined in a microwave vessel equipped with a teflon stirbar. The system wasflushed with argon. A degassed mixture of 3:1 acetone:water (2-3 mL) was added, and the reaction washeated in a microwave to 100 C for 30 min. The product was purified via silica gel chromatography inethyl acetate/hexanes.
 

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