There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 927-58-2 | MDL No. : | MFCD00000753 |
Formula : | C4H6BrClO | Boiling Point : | - |
Linear Structure Formula : | Br(CH2)3COCl | InChI Key : | LRTRXDSAJLSRTG-UHFFFAOYSA-N |
M.W : | 185.45 | Pubchem ID : | 70225 |
Synonyms : |
|
Signal Word: | Danger | Class: | 8 |
Precautionary Statements: | P210-P261-P264-P271-P280-P301+P330+P331-P303+P361+P353-P304+P340+P310-P305+P351+P338+P310-P363-P370+P378-P403+P233-P403+P235-P405-P501 | UN#: | 3265 |
Hazard Statements: | H227-H314-H335 | Packing Group: | Ⅱ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
86% | 4-Bromo-/V-quinolin-6-yl-butyramide (Intermediate compound); A mixture of 5-bromobuturylchloride (5.00 g, 25.6 mmol) and dichloromethane (50 ml) was cooled to 0C. 6-Aminoquinoline (3.43 g, 23.3 mmol) was added in small portions during 15 minutes. The temperature was allowed to reach room-temperature and stir for 15 h. Aqueous sodium hydroxide (40 ml, 1 M) was added and the mixture was extracted with dichloromethane (60 ml). The mixture was evaporated and diethylether (5 ml) was added, the solid was filtered and washed with diethylether. Yield 5.9 g (86%). |