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Chemical Structure| 92511-12-1 Chemical Structure| 92511-12-1

Structure of 92511-12-1

Chemical Structure| 92511-12-1

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CAS No.: 92511-12-1

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Product Details of [ 92511-12-1 ]

CAS No. :92511-12-1
Formula : C10H23IOSi
M.W : 314.28
SMILES Code : C[Si](OCCCCI)(C(C)(C)C)C
MDL No. :MFCD01863695
InChI Key :INGJYKISFRSCQV-UHFFFAOYSA-N
Pubchem ID :4250746

Safety of [ 92511-12-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302
Precautionary Statements:P280-P305+P351+P338

Application In Synthesis of [ 92511-12-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 92511-12-1 ]

[ 92511-12-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 161609-84-3 ]
  • [ 92511-12-1 ]
  • [ 959689-83-9 ]
YieldReaction ConditionsOperation in experiment
67% With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20℃; for 18.5h; Benzyl 4-(4-(tert-butyldimethylsilyloxy)butyl)-4-cyanopiperidine-1-carboxylate. To a stirred solution of <strong>[161609-84-3]benzyl 4-cyanopiperidine-1-carboxylate</strong> (10 g, 410 mmol) and iodo-tert-butyldimethylsilane butane (12.6 mL, 49 mmol) in THF (80 mL) cooled to -78 C. was added LiHMDS (50 mL, 50 mmol, 1M in THF) dropwise over 30 min. The resulting mixture was stirred while gradually warming to room temperature for 18 h. After quenching with water, the organic phase was diluted with EtOAc and washed with water, brine and dried (Na2SO4). After concentration, the residue was purified by flash chromatography (1% to 20% EtOAc/hexane) to give the title compound as yellow oil (11.88 g, 67% yield). 1H NMR (300 MHz, CDCl3) delta: 7.34-7.28 (5H, m), 5.09 (2H, s), 4.17 (2H, bs), 3.59 (2H, t, J=5.3 Hz), 3.07 (2H, bs), 1.89 (2H, d, J=13.2 Hz), 1.53 (6H, bs), 1.43-1.34 (2H, m), 0.85 (9H, s), 0.01 (6H, s). LCMS (M+H): 431.20.
 

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Related Functional Groups of
[ 92511-12-1 ]

Iodides

Chemical Structure| 78878-05-4

A307438 [78878-05-4]

tert-Butyl(3-iodopropoxy)dimethylsilane

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