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[ CAS No. 91-02-1 ] {[proInfo.proName]}

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Chemical Structure| 91-02-1
Chemical Structure| 91-02-1
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Product Details of [ 91-02-1 ]

CAS No. :91-02-1 MDL No. :MFCD00006300
Formula : C12H9NO Boiling Point : No data available
Linear Structure Formula :- InChI Key :GCSHUYKULREZSJ-UHFFFAOYSA-N
M.W : 183.21 Pubchem ID :7038
Synonyms :

Safety of [ 91-02-1 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P305+P351+P338 UN#:
Hazard Statements:H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 91-02-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 91-02-1 ]

[ 91-02-1 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 7504-94-1 ]
  • [ 91-02-1 ]
  • N-[1-Phenyl-1-pyridin-2-yl-meth-(E)-ylidene]-N'-pyrimidin-2-yl-hydrazine [ No CAS ]
  • 2
  • [ 38956-79-5 ]
  • [ 91-02-1 ]
  • N-(6-Methyl-pyridazin-3-yl)-N'-[1-phenyl-1-pyridin-2-yl-meth-(E)-ylidene]-hydrazine [ No CAS ]
  • 3
  • [ 91-02-1 ]
  • [ 7292-74-2 ]
  • 3-(3-fluorophenyl)-1-phenylimidazo[1,5-a]pyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
81% With di-tert-butyl peroxide; iodine; In toluene; at 120℃; for 12h;Sealed tube; General procedure: To a 10mL reaction tube were added L-Proline-MCM-41-Cu(OTf)2 (71mg, 0.045mmol), 2-benzoylpyridine 1 (0.3mmol), amino acid 2(0.9mmol), molecular iodine (0.045mmol), DTBP (0.75mmol), and toluene (2mL). The reaction tube was sealed and placed in an oil bath at room temperature. The reaction mixture was stirred at 120 C for 12 h. After being cooled to room temperature, the reaction mixture was diluted with 15 mL of EtOAc, and filtered. The L-Proline-MCM-41-Cu(OTf)2 complex was washed with EtOAc (25mL) and ethanol (2 5mL), and reused in the next run. The filtrate was concentrated in vacuo and the residue was purified by flash column chromatography on silica gel (petroleum ether: EtOAc 15:1-20:1) to provide the desired product 3.
  • 4
  • [ 91-02-1 ]
  • [ 475250-52-3 ]
  • 2-(4-methoxyphenyl)-1-phenyl-1-(pyridin-2-yl)ethan-1-ol [ No CAS ]
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