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Chemical Structure| 879551-04-9 Chemical Structure| 879551-04-9

Structure of 879551-04-9

Chemical Structure| 879551-04-9

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CAS No.: 879551-04-9

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Product Details of [ 879551-04-9 ]

CAS No. :879551-04-9
Formula : C6H9FO4
M.W : 164.13
SMILES Code : O=C1O[C@H](CO)[C@@H](O)[C@]1(F)C
MDL No. :MFCD23106443
InChI Key :VNCJYMKHJWVTPK-ZMIZWQJLSA-N
Pubchem ID :56605413

Safety of [ 879551-04-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H320-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 879551-04-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 879551-04-9 ]

[ 879551-04-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 349-43-9 ]
  • [ 15186-48-8 ]
  • [ 879551-04-9 ]
  • [ 1040882-61-8 ]
YieldReaction ConditionsOperation in experiment
Acetone-D-glyceraldehyde (39 g, 300 mmol) and <strong>[349-43-9]ethyl 2-fluoropropionate</strong> (54 g, 450 mmol) were dissolved in dry tetrahydrofuran (150 mL), and then the mixture was added dropwise to a tetrahydrofuransolution (300 mL) containing lithium diisopropylamide (510 mmol) at the temperature of no more than ?70 ° C. After the addition was complete, the temperature was gradually raised to room temperature. After stirring for 2 h, the reaction solution was poured into the saturated aqueous potassium dihydrogen phosphate solution (3000 mL). The organic solvent was evaporated by rotary evaporation. The residue was extracted with ethyl acetate, and concentrated to give an oily substance. Acetic acid (120 mL) and water (80 int) were added to the concentrated oily substance. The resulting mixture was heated in oil bath at 90 ° C. for 2 h, and then removing acetic acid and water by rotary evaporation. The residue was dehydrated twice with anhydrous ethanol (20 mL×2).Acetone (100 mL) was added to the residue, and then drying by evaporation again, so as to give an oily substance (70 g), i.e., 2-deoxy-2-fluoro-2-C-methyl-D-ribono-1,4-lactone mixture (Compound Aa).
 

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