Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 87-79-6 | MDL No. : | MFCD00151097 |
Formula : | C6H12O6 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | BJHIKXHVCXFQLS-OTWZMJIISA-N |
M.W : | 180.16 | Pubchem ID : | 6904 |
Synonyms : |
|
Chemical Name : | (3S,4R,5S)-1,3,4,5,6-Pentahydroxyhexan-2-one |
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
54% | With FAD; Staphylococcus carnosus D-fructose 1,6-bisphosphate aldolase; Streptococcus pneumonia glycerol phosphate oxidase; In water-d2; at 30℃; for 22h;pH 7;Enzymatic reaction; | General procedure: To a solution of DL-glycerol 3-phosphate magnesium salt (548.78 mg, 2.4 mmol) in 6.86 mL ddH2O was added <strong>[497-09-6]D-glyceraldehyde</strong> (or L-glyceraldehyde) (2 mL, 0.5 M, 1.0 mmol) at pH 7.0, glycerol phosphate oxidase saturated with FAD (final concentration 0.2 mg/mL), catalase (1000 U, 1.18 muL) and aldolase (final concentration 0.5 mg/mL). ddH2O was added to bring the total volume to 10 mL if necessary. The reaction mixture was shaken at 30 °C for 22 h and the reaction was monitored by TLC (developed by nBuOH/AcOH/H2O 2/1/1 (v/v/v) and stained with anisaldehyde sugar stain). The pH was then adjusted to pH ~5 with 6 N HCl and 11 muL acid phosphatase (18 U) was added and the mixture was shaken at 37 °C for 24 h. After cooling to rt., the pH was adjusted to 7.0 with 1 N NaOH and the mixture was diluted with methanol. The solution was filtered through Celite and washed with methanol. The filtrate was concentrated under reduced pressure and the residue was purified by silica gel column chromatography (EtOAc/iPrOH/H2O 9/3/1 (v/v/v)) to afford a pale yellow syrup which was further purified by Bio gel P-2 column. The mixture of monosaccharides could be isolated by Ca2+ exchange resin column. The purification process using P-2 column or Ca2+ exchange resin column was performed with the same procedure we previously used. |
28% | To a solution of DL-glycerol 3-phosphate magnesium salt (548.78 mg, 2.4 mmol) in 6.86 mL ddH2O were added <strong>[497-09-6]D-glyceraldehyde</strong> (or L-glyceraldehyde) (2 mL, 0.5 M, 1.0 mmol) at pH 7.0, glycerol phosphate oxidase (70 U, 2 mg), catalase (1000 U, 1.18 muL), and FruAS.car (final concentration 0.5 mg/mL). ddH2O was added to bring the total volume to 10 mL if necessary. The mixture was shaken at rt for 22 h and the reaction was monitored by TLC (developed by nBuOH/AcOH/H2O: 2/1/1 (v/v/v) and stained with anisaldehyde sugar stain). The pH was then adjusted to pH .similar.5 with 6 M HCl and 11 muL acid phosphatase (18 U) was added and the mixture was shaken at 37 °C for 24 h. After cooling to rt, the pH was adjusted to 7.0 with 1 M NaOH and the mixture was diluted with methanol. The solution was filtered through Celite and washed with methanol. The filtrate was concentrated under reduced pressure and the residue was purified by silica gel column chromatography (EtOAc/iPrOH/H2O: 9/3/1 (v/v/v)) to afford a pale yellow syrup which was further purified by Bio gel P-2 column. After purification, 108 mg d-fructose (60percent yield based on d-glyceraldehyde) and 50.9 mg l-sorbose (28percent yield based on l-glyceraldehyde) were obtained, respectively. |
[ 551-68-8 ]
(3R,4R,5R)-1,3,4,5,6-Pentahydroxyhexan-2-one
Similarity: 1.00
[ 57-48-7 ]
(3S,4R,5R)-1,3,4,5,6-Pentahydroxyhexan-2-one
Similarity: 1.00
[ 59-23-4 ]
(2R,3S,4S,5R)-2,3,4,5,6-Pentahydroxyhexanal
Similarity: 0.87
[ 39002-30-7 ]
(3S,4R,5R)-1-Amino-3,4,5,6-tetrahydroxyhexan-2-one hydrochloride
Similarity: 0.72
[ 527-07-1 ]
Sodium (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanoate
Similarity: 0.71
[ 551-68-8 ]
(3R,4R,5R)-1,3,4,5,6-Pentahydroxyhexan-2-one
Similarity: 1.00
[ 57-48-7 ]
(3S,4R,5R)-1,3,4,5,6-Pentahydroxyhexan-2-one
Similarity: 1.00
[ 59-23-4 ]
(2R,3S,4S,5R)-2,3,4,5,6-Pentahydroxyhexanal
Similarity: 0.87
[ 39002-30-7 ]
(3S,4R,5R)-1-Amino-3,4,5,6-tetrahydroxyhexan-2-one hydrochloride
Similarity: 0.72
[ 527-07-1 ]
Sodium (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanoate
Similarity: 0.71
[ 551-68-8 ]
(3R,4R,5R)-1,3,4,5,6-Pentahydroxyhexan-2-one
Similarity: 1.00
[ 57-48-7 ]
(3S,4R,5R)-1,3,4,5,6-Pentahydroxyhexan-2-one
Similarity: 1.00
[ 39002-30-7 ]
(3S,4R,5R)-1-Amino-3,4,5,6-tetrahydroxyhexan-2-one hydrochloride
Similarity: 0.72
[ 6705-49-3 ]
7-Oxabicyclo[4.1.0]heptan-2-one
Similarity: 0.70
[ 624734-17-4 ]
3-Methoxydihydro-2H-pyran-4(3H)-one
Similarity: 0.68