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CAS No. : | 824-75-9 | MDL No. : | MFCD00007992 |
Formula : | C7H6FNO | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | VNDHYTGVCGVETQ-UHFFFAOYSA-N |
M.W : | 139.13 | Pubchem ID : | 71572 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In N,N-dimethyl-formamide; at 145℃; for 16h; | INTERMEDIATE 344-[2-(4-Fluoropheny1H3-oxazol-4-yl]piperidineA solution of 4-fluorobenzamide (4.54 g, 32.7 mmol) and /-butyl 4-(bromoacetyl)-piperidine-1- carboxylate (5.0 g, 16.3 mmol) in DMF (40 mL) was heated at 145°C for 16 h. Upon completion of the reaction, the solution was allowed to cool to rt and concentrated to a dark oil. The oil was purified by reverse phase HPLC to afford the title compound (760 mg). LC/MS: m/e 247.08 (M+H).div.. | |
In N,N-dimethyl-formamide; at 145℃; for 16h; | A solution of 4-fluorobenzamide (4.54 g, 32.7 mmol) and t-butyl 4-(bromoacetyl)-piperidine-1-carboxylate (5.0 g, 16.3 mmol) in DMF (40 mL) was heated at 145'C for 16 h. Upon completion of the reaction, the solution was allowed to cool to rt and concentrated to a dark oil. The oil was purified by reverse phase HPLC to afford the title compound (760 mg). LC/MS: m/e 247.08 (M+14)+. |