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Chemical Structure| 766-77-8 Chemical Structure| 766-77-8

Structure of Dimethylphenylsilane
CAS No.: 766-77-8

Chemical Structure| 766-77-8

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CAS No.: 766-77-8

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Product Details of [ 766-77-8 ]

CAS No. :766-77-8
Formula : C8H12Si
M.W : 136.27
SMILES Code : C[SiH](C)C1=CC=CC=C1
MDL No. :MFCD00008257
InChI Key :OIKHZBFJHONJJB-UHFFFAOYSA-N
Pubchem ID :6327656

Safety of [ 766-77-8 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H225
Precautionary Statements:P210-P233-P240-P241-P242-P243-P280-P303+P361+P353-P370+P378-P403+P235-P501
Class:3
UN#:1993
Packing Group:Ⅱ

Application In Synthesis of [ 766-77-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 766-77-8 ]

[ 766-77-8 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 766-77-8 ]
  • [ 71902-33-5 ]
  • 1-dimethylphenylsilyl-3,5-difluoro-1,4-dihydropyridine [ No CAS ]
  • 2
  • [ 27829-72-7 ]
  • [ 766-77-8 ]
  • ethyl 2-[dimethyl(phenyl)silyl]hexanoate [ No CAS ]
  • 3
  • [ 106-86-5 ]
  • [ 766-77-8 ]
  • [ 20988-14-1 ]
YieldReaction ConditionsOperation in experiment
General procedure: In a typical procedure, styrene, hydrosilane and the catalyst (1:1:0.03 M ratio) were dissolved in dry toluene and heated in a Schlenk bomb flask fitted with a plug valve at 80 C for 30 min. Next, 0.12 equiv. of NaHBEt3 was added and the reaction mixture was again heated for 2-24 h at 80 C (Table 1).
  • 4
  • [ 393-56-6 ]
  • [ 766-77-8 ]
  • 4-(dimethyl(phenyl)silyl)-2-fluoro-N,N-dimethylaniline [ No CAS ]
  • 5
  • [ 766-77-8 ]
  • [ 22259-53-6 ]
  • (2-(dimethyl(phenyl)silyl)-1H-indol-3-yl)methanamine [ No CAS ]
  • 6
  • [ 769-26-6 ]
  • [ 766-77-8 ]
  • (mesitylethynyl)dimethyl(phenyl)silane [ No CAS ]
YieldReaction ConditionsOperation in experiment
86% With sodium hydroxide; In 1,2-dimethoxyethane; at 25℃; for 24h;Inert atmosphere; Glovebox; Sealed tube; The general procedure was followed. The reaction was performed with NaOH (2.0 mg, 0.05 mmol, 10 mol %), <strong>[769-26-6]2-ethynyl-1,3,5-trimethylbenzene</strong> (57 mg, 0.5 mmol, 1.0 equiv), PhMe2SiH (204 mg, 230 μL, 1.5 mmol, 3.0 equiv), and 0.5 mL of 1,2-dimethoxyethane (DME) at 25 C. for 24 h. The desired product 4i (119.1 mg, 86% yield) was obtained as a colorless oil after solvent removal at 85 C. at 45 mtorr for 30 minutes. 1H NMR (500 MHz, CDCl3) δ 7.73 (ddt, J=4.5, 3.2, 0.8 Hz, 3H), 7.40 (dd, J=2.5, 0.8 Hz, 2H), 6.88-6.86 (m, 2H), 2.42 (s, 6H), 2.29 (s, 3H), 0.52 (t, J=0.7 Hz, 6H); 13C NMR (126 MHz, CDCl3) δ 140.86, 138.23, 137.66, 133.89, 129.45, 127.99, 127.67, 119.94, 104.95, 99.66, 21.51, 21.15, -0.34. IR (Neat Film NaCl) 3440, 3068, 2959, 2146, 1646, 1610, 1474, 1428, 1224, 1117, 841, 825, 779, 753, 698 cm-1; HRMS (EI+) calc'd for C19H23Si [M+H]: 279.1569. found 279.1561.
  • 7
  • [ 766-77-8 ]
  • [ 2914-69-4 ]
  • (S,E)-4-(dimethyl(phenyl)silyl)but-3-en-2-ol [ No CAS ]
  • (R,E)-4-(dimethyl(phenyl)silyl)but-3-en-2-ol [ No CAS ]
  • 8
  • [ 766-77-8 ]
  • [ 113486-06-9 ]
  • tert-butyl {(3E)-4-[dimethyl(phenyl)silyl]-2-methylbut-3-en-2-yl}carbamate [ No CAS ]
 

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