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CAS No. : | 7328-91-8 | MDL No. : | MFCD00009801 |
Formula : | C5H14N2 | Boiling Point : | No data available |
Linear Structure Formula : | C(CH3)2(CH2NH2)2 | InChI Key : | DDHUNHGZUHZNKB-UHFFFAOYSA-N |
M.W : | 102.18 | Pubchem ID : | 81770 |
Synonyms : |
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Signal Word: | Danger | Class: | 8,3 |
Precautionary Statements: | P280-P305+P351+P338-P310 | UN#: | 2920 |
Hazard Statements: | H226-H314 | Packing Group: | Ⅱ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In DMF (N,N-dimethyl-formamide); at 100℃; for 5h; | A solution of <strong>[31872-62-5]4-methoxy-3-nitropyridine</strong> (5.00 g, 32.4 MMOL) and 2,2- dimethyl-1, 3-propanediamine (16.2 g, 161 MMOL) in DMF (100 mL) was heated at 100 °C for 5 h. The solvent was removed under reduced pressure to give 7.30 g of the desired COMPOUND. 1H NMR (400 MHz, CDCL3) 8 9.20 (s, 2H), 9.10 (br, 1H), 8.20 (d, 1H), 6.70 (d, 1 H), 3.25 (d, 2H), 2.60 (s, 2H), 1.25 (br, 2H), 0.95 (s, 6H). |