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CAS No. : | 7098-07-9 | MDL No. : | MFCD00055389 |
Formula : | C5H8N2 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | IWDFHWZHHOSSGR-UHFFFAOYSA-N |
M.W : | 96.13 | Pubchem ID : | 81540 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P280 | UN#: | |
Hazard Statements: | H302+H312+H332 | Packing Group: | |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In acetonitrile; at 38℃; for 24h; | General procedure: According to the method provided in the literature [27], firstly,under the protection of argon 1-ethylimidazole and 2-bromoethylmethyl ether were mixed and acetonitrile was added asthe reaction solvent, then reflux reaction at 38 C for 24 h. Colorless liquidcrude products were washed and extracted with ethyl ether andthen dried in vacuumdrying box for 48 h after rotary evaporation to obtainintermediate product [C22O1IM][Br]. And the [C22O1IM][Br] wascharacterized by 1HNMR (see Fig. S1 of the Supporting Information).The attribution of chemical displacement, integral area and formant ofcorresponding groups is shown in Table S2. The synthesis route isshown in the Scheme 1. |
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