Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 698-01-1 | MDL No. : | MFCD03452792 |
Formula : | C8H10ClN | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | QDCPXCIPVQJVDD-UHFFFAOYSA-N |
M.W : | 155.63 | Pubchem ID : | 12772 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
36%; 63% | With NaY-BS zeolite; at 150℃; for 1h; | General procedure: Into a pressure microreactor of stainless steel of 17 mL capacity or into a glass ampule (20 mL) (results of the parallel runs were virtually identic) was charged 5-10 wt % of catalyst (0.94HY-BS, NaY-BS, 0.72KNaX-BS), 100 mmol of aniline or its derivative, and 400 mmol of dimethyl carbonate. The reactor was hermetically closed (the ampule was sealed), and was heated for 1-4 h at 150 C. After the end of the run the reactor was cooled to room temperature, opened, the reaction mixture was filtered through a bed of Al2O3. Dimethyl carbonate was distilled off, the residue was distilled at atmospheric pressure or in a vacuum, or crystallized from ethanol. |
55%; 38% | With 0.72 KNaX-BS zeolite; at 150℃; for 1h; | General procedure: Into a pressure microreactor of stainless steel of 17 mL capacity or into a glass ampule (20 mL) (results of the parallel runs were virtually identic) was charged 5-10 wt % of catalyst (0.94HY-BS, NaY-BS, 0.72KNaX-BS), 100 mmol of aniline or its derivative, and 400 mmol of dimethyl carbonate. The reactor was hermetically closed (the ampule was sealed), and was heated for 1-4 h at 150 C. After the end of the run the reactor was cooled to room temperature, opened, the reaction mixture was filtered through a bed of Al2O3. Dimethyl carbonate was distilled off, the residue was distilled at atmospheric pressure or in a vacuum, or crystallized from ethanol. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With methanol; hydrogen; at 99.84℃; under 9750.98 Torr; for 2.11667h;Autoclave; | General procedure: The catalytic hydrogenation reaction was conducted in a stainless-steel autoclave reactor (70mL capacity) heated in oil bath. Substrate (6mmol), solvent (20mL) and catalyst (0.5g) were directly added into the reactor. The autoclave was purged with N2 and H2 three times before the reaction started. The reaction process was monitored by gas chromatography (GC) (Agilent 6890) with a flame ionization detector (FID) system. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
6% | With zirconium(IV) chloride; N-fluorobis(benzenesulfon)imide; In chloroform; for 5.0h;Reflux; | General procedure: To a solution of amine (0.1mmol) in 3mL of CHCl3 the corresponding amount of NFSI in 2mL of the same solvent was added. The reaction mass was stirred at selected temperature during the time indicated in Table 1. The resulting solution was washed with water (2×15mL), dried over Na2SO4 and evaporated to dryness. The residue was analyzed either by GC/MS or separated by column chromatography. |
[ 16154-72-6 ]
3-Chloro-4-(4-methylpiperazin-1-yl)benzenamine
Similarity: 0.89
[ 1052538-72-3 ]
3-Chloro-4-(4-methylpiperazin-1-yl)aniline hydrochloride
Similarity: 0.89
[ 16154-72-6 ]
3-Chloro-4-(4-methylpiperazin-1-yl)benzenamine
Similarity: 0.89
[ 1052538-72-3 ]
3-Chloro-4-(4-methylpiperazin-1-yl)aniline hydrochloride
Similarity: 0.89
[ 16154-72-6 ]
3-Chloro-4-(4-methylpiperazin-1-yl)benzenamine
Similarity: 0.89
[ 1052538-72-3 ]
3-Chloro-4-(4-methylpiperazin-1-yl)aniline hydrochloride
Similarity: 0.89