Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 69610-41-9 | MDL No. : | MFCD00274186 |
Formula : | C10H17NO3 | Boiling Point : | No data available |
Linear Structure Formula : | (CH3)3COC(O)(NC4H7)C(O)H | InChI Key : | YDBPZCVWPFMBDH-QMMMGPOBSA-N |
M.W : | 199.25 | Pubchem ID : | 2734674 |
Synonyms : |
|
Chemical Name : | (S)-1-Boc-2-Formylpyrrolidine |
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P321-P332+P313-P337+P313-P362-P403+P233-P405-P501 | UN#: | |
Hazard Statements: | H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Example 87A (S)-N-Boc-2-Formyl-pyrrolidine STR115 (S)-N-Boc-2-Formyl-pyrrolidine was prepared by Swern oxidation of (S)-N-Boc prolinol (Fluka) according to the conditions described by M. G. B. Drew et al., J. Chem. Soc. Perkin 1, 1998, 1627, for the oxidation of CBZ-prolinol. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
90% | With ammonium acetate; In dimethyl sulfoxide; at 60℃; for 2h; | The compound DSV102 (2.63g) and dimethyl sulfoxide (30ml) were added to a 50ml three-necked flask, and reacted at 30 C for 31 hours.Ammonium acetate (2.31 g), L-Boc guanaldehyde (1.99 g), and reacted at 60 C for 2 h. Add 30ml of anhydrous methanol dropwise, stir at 25 CAt night (14h), suction filtration, solid washing with water (20ml * 3), drying at 80 C under vacuum, to obtain 2.81g solid DSV01, yield 90%,The purity is 96%. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
85% | With ammonium acetate; In dimethyl sulfoxide; at 30℃; for 4h; | Add to a 100ml two-neck bottleBrominated biphenyl diacetyl(1.98g),Dimethyl sulfoxide (20ml),The reaction was carried out at 25 C for 16 h, and ammonium acetate (2.31 g) was added.L-Boc-prolinal(1.99 g), reacted at 30 C for 4 h.Add 20 ml of anhydrous methanol, 20 ml of water, and stir for 45 min.Filter by suction, wash the solid with water (20ml * 3), vacuum dry at 80 C,Obtained 2.66 g of solid DSV01,The yield is 85%,The purity is 94%. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
82% | Add DSV101 (1.54g) to a 50ml three-necked flask,Potassium bromide (0.30 g), dimethyl sulfoxide (10 ml),After reacting at 75 C for 6 h, the temperature was lowered, and ammonium acetate (2.31 g) was added.L-Boc guanylaldehyde (1.99 g) was reacted at 40 C for 5 h. Add 100ml of water,The organic layer was washed with brine (100 ml)Separation by column chromatography2.56g solid DSV01,The yield is 82%.The purity is 95% |
[ 54503-10-5 ]
tert-Butyl 2-carbamoylpyrrolidine-1-carboxylate
Similarity: 0.90
[ 15761-39-4 ]
(S)-1-(tert-Butoxycarbonyl)pyrrolidine-2-carboxylic acid
Similarity: 0.88