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[ CAS No. 69360-26-5 ] {[proInfo.proName]}

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Chemical Structure| 69360-26-5
Chemical Structure| 69360-26-5
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Product Details of [ 69360-26-5 ]

CAS No. :69360-26-5 MDL No. :MFCD00052341
Formula : C7H4ClNO2S Boiling Point : -
Linear Structure Formula :- InChI Key :NQAYCMBZPAARNO-UHFFFAOYSA-N
M.W : 201.63 Pubchem ID :522347
Synonyms :

Safety of [ 69360-26-5 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:3261
Hazard Statements:H314 Packing Group:Ⅱ
GHS Pictogram:

Application In Synthesis of [ 69360-26-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 69360-26-5 ]

[ 69360-26-5 ] Synthesis Path-Downstream   1~6

  • 1
  • [ 881674-56-2 ]
  • [ 69360-26-5 ]
  • [ 881677-06-1 ]
YieldReaction ConditionsOperation in experiment
77% Reference Example 242 2-[2-(2-Fluorophenyl)-4-formyl-1H-pyrrol-1-yl]sulfonyl}benzonitrile To a solution (28 mL) of <strong>[881674-56-2]5-(2-fluorophenyl)-1H-pyrrole-3-carbaldehyde</strong> (284 mg) in tetrahydrofuran was added sodium hydride (60% in oil, 181 mg) at room temperature and the mixture was stirred for 30 min. 15-Crown-5 (992 mg) was added dropwise and the mixture was stirred for 30 min, (2-cyanobenzene)sulfonyl chloride (606 mg) was added, and the mixture was further stirred for 1 hr. Saturated brine was added to the reaction mixture, and the mixture was extracted with ethyl acetate. The extract was washed with saturated brine, dried over anhydrous magnesium sulfate, and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (eluent: hexane-ethyl acetate=4:1?2:3) to give the title compound as colorless crystals (yield 410 mg, 77%). 1H-NMR (CDCl3)delta: 6.70 (1H, d, J=1.7 Hz), 6.83-6.89 (1H, m), 7.08-7.18 (2H, m), 7.32-7.52 (3H, m), 7.70-7.75 (1H, m), 7.82-7.85 (1H, m), 8.39 (1H, d, J=1.7 Hz), 9.94 (1H, s).
In tetrahydrofuran; Reference Example 242 2-[2-(2-Fluorophenyl)-4-formyl-1H-pyrrol-1-yl]sulfonyl}benzonitrile To a solution (28 mL) of <strong>[881674-56-2]5-(2-fluorophenyl)-1H-pyrrole-3-carbaldehyde</strong> (284 mg) in tetrahydrofuran was added sodium hydride (60% in oil, 181 mg) at room temperature and the mixture was stirred for 30 min. 15-Crown-5 (992 mg) was added dropwise and the mixture was stirred for 30 min, (2-cyanobenzene)sulfonyl chloride (606 mg) was added, and the mixture was further stirred for 1 hr. Saturated brine was added to the reaction mixture, and the mixture was extracted with ethyl acetate. The extract was washed with saturated brine, dried over anhydrous magnesium sulfate, and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (eluent: hexane-ethyl acetate=4:1?2:3) to give the title compound as colorless crystals (yield 410 mg, 77%). 1H-NMR (CDCl3)delta: 6.70 (1H, d, J=1.7 Hz), 6.83-6.89 (1H, m), 7.08-7.18 (2H, m), 7.32-7.52 (3H, m), 7.70-7.75 (1H, m), 7.82-7.85 (1H, m), 8.39 (1H, d, J=1.7 Hz), 9.94 (1H, s).
  • 2
  • [ 69360-26-5 ]
  • [ 33537-99-4 ]
  • 2-((6-chloro-3,4-dihydroisoquinolin-2(1H)-yl)sulfonyl)benzonitrile [ No CAS ]
  • 3
  • [ 69360-26-5 ]
  • [ 33537-99-4 ]
  • (E)-ethyl 3-(6-chloro-2-((2-cyanophenyl)sulfonyl)-1,2,3,4-tetrahydroisoquinolin-8-yl)acrylate [ No CAS ]
  • C21H19ClN2O4S [ No CAS ]
  • 4
  • [ 82771-60-6 ]
  • [ 69360-26-5 ]
  • 2-((7-chloro-3,4-dihydroisoquinolin-2(1H)-yl)sulfonyl)benzonitrile [ No CAS ]
  • 5
  • [ 82771-60-6 ]
  • [ 69360-26-5 ]
  • (E)-ethyl 3-(7-chloro-2-((2-cyanophenyl)sulfonyl)-1,2,3,4-tetrahydroisoquinolin-8-yl)acrylate [ No CAS ]
  • (E)-ethyl 3-(7-chloro-2-((2-cyanophenyl)sulfonyl)-1,2,3,4-tetrahydroisoquinolin-6-yl)acrylate [ No CAS ]
  • 6
  • [ 69360-26-5 ]
  • [ 33084-49-0 ]
  • 2-cyano-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
70% EXAMPLE 78 2-Cyano-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide 2-Cyano-N-(4-bromo-3-methyl-5-isoxazolyl)benzenesulfonamide was prepared from <strong>[33084-49-0]5-amino-4-bromo-3-methylisoxazole</strong> and 4-chlorobenzenesulfonyl chloride according to the procedures described in Example 45. The crude product was purified by recrystallization from ethyl acetate/hexanes to give a crystalline solid, m.p. 152-155 C., yield 70%.
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