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Chemical Structure| 68716-47-2 Chemical Structure| 68716-47-2
Chemical Structure| 68716-47-2

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CAS No.: 68716-47-2

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Product Details of [ 68716-47-2 ]

CAS No. :68716-47-2
Formula : C6H5BCl2O2
M.W : 190.82
SMILES Code : C1=CC(=CC(=C1B(O)O)Cl)Cl
MDL No. :MFCD00013930
InChI Key :QNEGDGPAXKYZHZ-UHFFFAOYSA-N
Pubchem ID :2734659

Safety of [ 68716-47-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis [ 68716-47-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 68716-47-2 ]

[ 68716-47-2 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 19240-91-6 ]
  • [ 68716-47-2 ]
  • [ 74298-93-4 ]
  • 2
  • [ 845751-59-9 ]
  • [ 68716-47-2 ]
  • [ 845751-61-3 ]
YieldReaction ConditionsOperation in experiment
83% EXAMPLE 2 7- (2,4-Dichloro-phenyl)-2-methyl-2H-indazole 5 : Ar = 2,4-dichlorophenyl ; R = Me step 1 A solution OF 7-BROMO-LH-INDAZOLE (3; 1.01 g, 5.13 mmol) and tetrakis (triphenylphosphine) palladium (0) (0.176 g, 0.152 mmol) in 15 mL of ethylene glycol dimethyl ether was stirred for 30 m. To the solution was added 2,4-dichlorophenyl boronic acid (1.93 g, 10.1 mmol) and a 2 M aqueous NA2CO3 solution (7.1 mL, 14.2 mmol). The orange-yellow mixture was stirred at 80 C for 19 h, allowed to cool, and then partitioned between 50 mL of ethyl acetate and 50 mL of water. The organic layer was dried over MGS04, filtered, and concentrated to an orange oil. Column chromatography (0O10% EtOAc/hexanes) afforded OF 7-(2, 4-DICHLORO-PHENYL)-LH- indazole as a pale yellow foamy solid (4; 1.12 g, 83%).
  • 3
  • [ 38411-20-0 ]
  • [ 68716-47-2 ]
  • [ 68194-05-8 ]
 

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