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CAS No. : | 6843-66-9 | MDL No. : | MFCD00025690 |
Formula : | C14H16O2Si | Boiling Point : | - |
Linear Structure Formula : | (C6H5)2Si(OCH3)2 | InChI Key : | AHUXYBVKTIBBJW-UHFFFAOYSA-N |
M.W : | 244.36 | Pubchem ID : | 81284 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280 | UN#: | N/A |
Hazard Statements: | H315 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
78.3% | In diethyl ether; at 40℃; for 3.5h;Inert atmosphere; | General procedure: Add petroleum ether as a solvent in a three-necked flask, first add 1 mol of diphenyldichlorosilane, mix well, pass1.5 mol of methanol and 0.3 mol of sodium methoxide were added to the flask under nitrogen atmosphere to maintain the environment, and the reaction was carried out at 40 C.After the GC monitors the consumption of diphenyldichlorosilane by about 40%, 0.3 mol of sodium methoxide is added to the reaction system to continue the reaction.The reaction was carried out for about 3.5 hours. After the reaction is completed, the reaction product is collected, filtered, and subjected to atmospheric distillation to obtain an alcoholysis product diphenyl.Dimethoxysilane, the yield was 93.77 |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
99% | With potassium hexamethylsilazane; In neat liquid; at 30℃; for 2h;Schlenk technique; Inert atmosphere; | General procedure: Catalyzed CDC reactions were carried out using the following standard protocol. In the glove box, the chosen pre-catalyst (0.05 mmol) was loaded into a Schlenk tube, and subsequently the alcohol (n x 0.05 mmol, n equiv.) followed by silane (n' x 0 0.05 mmol, n' equiv.) were added. The reaction mixture was stirred at the desired temperature (30C), which was controlled by an oil bath. After the required period, the reaction was quenched by adding CDCl3 to the mixture. Substrate conversion was monitored by examination of the 1H NMR spectrum of the reaction mixture and comparing relative intensities of resonance characteristics of the substrates and products. |
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