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Chemical Structure| 670-96-2 Chemical Structure| 670-96-2
Chemical Structure| 670-96-2

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CAS No.: 670-96-2

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2-Phenyl-1H-imidazole is an imidazole derivative used as a drug precursor for developing anti-infective and anti-inflammatory agents.

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Product Details of 2-Phenyl-1H-imidazole

CAS No. :670-96-2
Formula : C9H8N2
M.W : 144.17
SMILES Code : C1(C2=CC=CC=C2)=NC=CN1
MDL No. :MFCD00005186
InChI Key :ZCUJYXPAKHMBAZ-UHFFFAOYSA-N
Pubchem ID :69591

Safety of 2-Phenyl-1H-imidazole

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of 2-Phenyl-1H-imidazole

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 670-96-2 ]

[ 670-96-2 ] Synthesis Path-Downstream   1~8

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  • [ 2314-97-8 ]
  • [ 33469-36-2 ]
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  • [ 755039-55-5 ]
  • [ 1313518-37-4 ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate;trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; In 1,2-dimethoxyethane; at 200℃; for 2.0h;microwave irradiation; A mixture of intermediate B (50 mg, 0.17 mmol), 2-phenyl-lH-imidazole (3.4 mmol, 20 equivalents, 490 mg), Cul (0.05 equivalents, 0.009 mmol, 1.7 mg), trans- l,2-bis(methylamino)cyclohexane (14.2 mg, 0.003 mL) and K2CO3 (1.7 mmol, 233 mg) in 2 mL of DME were heated in a microwave at 200 C for 2h. The reaction was diluted with DME, filtered through Celite and evaporated. The residue was purified by reverse phase HPLC using a gradient of 30-50% CH3CN (0.1% TFA) over 30 min with a flow rate of 20 mL/min eluting from a PCRP-5 column (2.5 x 30 cm). Following lyophylization, 22.8 mg of the title compound was obtained with a purity > 99%. ? NMR (CDCI3) delta: 7.9-7.3 (m, 8H), 4.2 (m, 1H), 3.55 (m, 1H), 3.3 (s, 3H), 2.0-1.1 (m, 10H) and 0.85 ppm (t, 3H); LCMS: 403.2 m/z (M+H)+; ret. Time: 3.77 min (Analytical Method A).
  • 3
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  • [ 14651-42-4 ]
  • [ 1415725-27-7 ]
  • 4
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  • [ 57310-39-1 ]
  • 6-methylimidazo[1,2-f]phenanthridine [ No CAS ]
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  • [ 2926-30-9 ]
  • [ 33469-36-2 ]
  • 6
  • [ 13534-90-2 ]
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  • C14H9N3 [ No CAS ]
  • 7
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  • [ 77332-79-7 ]
  • C14H9N3 [ No CAS ]
  • 8
  • [ 4278-08-4 ]
  • [ 670-96-2 ]
 

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