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CAS No. : | 651-06-9 | MDL No. : | MFCD00006067 |
Formula : | C11H12N4O3S | Boiling Point : | - |
Linear Structure Formula : | NH2C6H4SO2NHC4N2H2OCH3 | InChI Key : | GPTONYMQFTZPKC-UHFFFAOYSA-N |
M.W : | 280.30 | Pubchem ID : | 5326 |
Synonyms : |
Sulfametoxydiazine;5-Methoxysulfadiazine;I-2586;Solfametossidiazina [DCIT];Sulfametoxipirimidine;SH 613;Sulfamethoxydiazine;NSC 683528;Bayrena
|
Chemical Name : | 4-Amino-N-(5-methoxypyrimidin-2-yl)benzenesulfonamide |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
97% | With 2,4-dichlorophenoxyacetic acid dimethylamine; | Example 105 N-[4-[(5-Methoxypyrimidin-2-yl)aminosulfonyl]phenyl]-(2-chloro-5-nitrophenyl)carboxamide The title compound (0.377 g, yield 97%) was obtained according to the procedure described in Example 2 using <strong>[651-06-9]sulfameter</strong> (a product of Sigma, 0.280 g, 1.0 mmol), DMA (2.5 ml) and 2-chloro-5-nitrobenzoyl chloride (0.264 g, 1.2 mmol). Rf 0.71 [methylenchloride:methanol=7:1 (v/v)]; 1H-NMR (400 MHz, DMSO-d6, TMS): delta(ppm) 3.80 (3H, s), 7.87 (2H, d, J=8.8 Hz), 7.91 (1H, d, J=8.8 Hz), 7.98 (2H, d, J=8.8 Hz), 8.30 (2H, s), 8.36 (1H, dd, J=2.2, 8.8 Hz), 8.52 (1H, d, J=2.2 Hz), 11.09 (1H, s), 11.46 (1H, br); MS(FAB) m/z: 464 (M+H)+. |
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