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Chemical Structure| 645-13-6 Chemical Structure| 645-13-6

Structure of 645-13-6

Chemical Structure| 645-13-6

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CAS No.: 645-13-6

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Product Details of [ 645-13-6 ]

CAS No. :645-13-6
Formula : C11H14O
M.W : 162.23
SMILES Code : CC(C1=CC=C(C(C)C)C=C1)=O
MDL No. :MFCD00048297
Boiling Point : No data available
InChI Key :PDLCCNYKIIUWHA-UHFFFAOYSA-N
Pubchem ID :12578

Safety of [ 645-13-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 645-13-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 645-13-6 ]

[ 645-13-6 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 7446-70-0 ]
  • [ 98-82-8 ]
  • [ 107-06-2 ]
  • [ 75-36-5 ]
  • [ 645-13-6 ]
  • [ 40428-87-3 ]
  • 3
  • [ 99-90-1 ]
  • [ 77047-87-1 ]
  • [ 2932-65-2 ]
  • [ 645-13-6 ]
  • 4
  • [ 23152-99-0 ]
  • [ 645-13-6 ]
YieldReaction ConditionsOperation in experiment
83% With hydrogenchloride; water; copper(l) chloride; In methanol; at 20℃; for 6h;Irradiation; Inert atmosphere; General procedure: A 10 mL reaction vessel with a magnetic stirring bar was equipped with phenylacetylene (1 mmol), CuCl (1 mol%), HCl (0.2 mL, 37 wt %) and methanol (2 mL). The mixture was irradiated with a blue LED (5 W) and stirred under at r.t. in an air atmosphere for 6 h. The distance of the reaction vial from the light is about 2 centimeter. After the reaction, the solvent was removed under reduced pressure. Purification of the crude product was achieved by flash column chromatography using petrol ether/ethyl acetate (6:1~10:1) as eluent.
 

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