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Chemical Structure| 642-71-7 Chemical Structure| 642-71-7
Chemical Structure| 642-71-7

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CAS No.: 642-71-7

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Antiarol is a member of aromatic phenols and exhibits moderate DPPH free radical scavenging activity.

Synonyms: 3,4,5-Trimethoxyphenol; 5-HYDROXY-1,2,3-TRIMETHOXYBENZENE

4.5 *For Research Use Only !

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Product Details of Antiarol

CAS No. :642-71-7
Formula : C9H12O4
M.W : 184.19
SMILES Code : OC1=CC(OC)=C(OC)C(OC)=C1
Synonyms :
3,4,5-Trimethoxyphenol; 5-HYDROXY-1,2,3-TRIMETHOXYBENZENE
MDL No. :MFCD00008389
InChI Key :VTCDZPUMZAZMSB-UHFFFAOYSA-N
Pubchem ID :69505

Safety of Antiarol

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of Antiarol

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 642-71-7 ]

[ 642-71-7 ] Synthesis Path-Downstream   1~5

  • 2
  • [ 642-71-7 ]
  • [ 71486-53-8 ]
  • [ 86370-97-0 ]
YieldReaction ConditionsOperation in experiment
EXAMPLE 3 1,2,3,4-Tetrahydro-8,9,10-trimethoxy-5H-[1]benzopyrano[3,4-c]pyridin-5-one hydrochloride Prepared by the method described in Example 1 from 3,4,5-trimethoxyphenol (25 g, 0.14 moles) and <strong>[71486-53-8]methyl 4-oxo-3-piperidinecarboxylate hydrochloride</strong> (18.8 g, 0.097 moles). Recrystallization from dilute aqueous hydrochloric acid yielded the product (17.5 g) as the hydrochloride, mp 232°-234° C.
  • 3
  • [ 642-71-7 ]
  • [ 52022-77-2 ]
  • 1,2,3-Trimethoxy-5-[2-(3-nitro-phenyl)-ethoxy]-benzene [ No CAS ]
  • 4
  • [ 642-71-7 ]
  • [ 2896-67-5 ]
  • C17H20O6 [ No CAS ]
  • 5
  • [ 642-71-7 ]
  • [ 1835-65-0 ]
  • C44H44N2O16 [ No CAS ]
YieldReaction ConditionsOperation in experiment
85% With potassium carbonate; In N,N-dimethyl-formamide; at 110℃; for 13h;Inert atmosphere; Under a nitrogen atmosphere, A-1 three-necked flask 1000ml (27mmol), potassium carbonate (407mmol), 3,4,5-trimethoxy phenol (A-15) (271mmol), put in DMF (150ml), 13 hours reaction is at 110 It was.Thereafter, by filtration, to remove the potassium carbonate.After evaporation of the solvent, AxisExtracted with Rorometan, washed with 10percent aqueous potassium hydroxide solution, dried over sodium sulfate.ItsAfter, the solvent was distilled off, column purification (dichloromethane: acetone = 10: 1) to be performedRi, to give compound A-16 (23mmol, 85percent)
 

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