98.0%(GC)| A1458434|Formula:C13H26O2|Molecular Weight:214.344350000+ products instock " />

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Chemical Structure| 638-53-9 Chemical Structure| 638-53-9
Chemical Structure| 638-53-9

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CAS No.: 638-53-9

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NSC 25955 is an endogenous metabolite.

Synonyms: N-Tridecanoic acid; C13:0 Fatty acid; n-Tridecoic acid

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Product Details of Tridecanoic Acid

CAS No. :638-53-9
Formula : C13H26O2
M.W : 214.34
SMILES Code : CCCCCCCCCCCCC(O)=O
Synonyms :
N-Tridecanoic acid; C13:0 Fatty acid; n-Tridecoic acid
MDL No. :MFCD00002741
InChI Key :SZHOJFHSIKHZHA-UHFFFAOYSA-N
Pubchem ID :12530

Safety of Tridecanoic Acid

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P305+P351+P338

Application In Synthesis of Tridecanoic Acid

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 638-53-9 ]

[ 638-53-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 25077-25-2 ]
  • [ 638-53-9 ]
  • 2
  • prolinol ester [ No CAS ]
  • [ 638-53-9 ]
  • [ 498-63-5 ]
  • [ 3554-65-2 ]
YieldReaction ConditionsOperation in experiment
With sodium hydrogencarbonate;toluene-4-sulfonic acid; In benzene; The resulting N-methyl<strong>[498-63-5]prolinol</strong> (3.0 g; 0.026 mol) was mixed with 5.6 g (0.026 mol) of tridecanoic acid, and a catalytic amount of p-toluenesulfonic acid was added thereto. The reaction mixture was azeotripically dehydrated in benzene for 3 hours. A saturated aqueous solution of sodium bicarbonate was added to the reaction mixture, and the mixture was extracted with benzene. The benzene extract was washed successively with water and a saturated sodium chloride aqueous solution, and dried over sodium sulfate. The benzene was removed by distillation, and the residue was purified by column chromatography to obtain 6.1 g (yield: 39percent from <strong>[498-63-5]prolinol</strong>) of a <strong>[498-63-5]prolinol</strong> ester of formula (II) wherein R3 =CH3 and R4 =-(CH2)11 CH3.
With sodium hydrogencarbonate;toluene-4-sulfonic acid; In benzene; The resulting N-methyl<strong>[498-63-5]prolinol</strong> (3.0 g; 0.026 mol) was mixed with 5.6 g (0.026 mol) of tridecanoic acid, and a catalytic amount of p-toluenesulfonic acid was added thereto. The reaction mixture was azeotripically dehydrated in benzene for 3 hours. A saturated aqueous solution of sodium bicarbonate was added to the reaction mixture, and the mixture was extracted with benzene. The benzene extract was washed successively with water and a saturated sodium chloride aqueous solution, and dried over sodium sulfate. The benzene was removed by distillation, and the residue was purified by column chromatography to obtain 6.1 g (yield: 39percent from <strong>[498-63-5]prolinol</strong>) of a <strong>[498-63-5]prolinol</strong> ester of formula (II) wherein R3 = CH3 and R4 = -(CH2)11CH3.
 

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