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[ CAS No. 6324-72-7 ] {[proInfo.proName]}

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Chemical Structure| 6324-72-7
Chemical Structure| 6324-72-7
Structure of 6324-72-7 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 6324-72-7 ]

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Product Details of [ 6324-72-7 ]

CAS No. :6324-72-7 MDL No. :MFCD00075623
Formula : C5H5N5OS Boiling Point : -
Linear Structure Formula :- InChI Key :JHEKNTQSGTVPAO-UHFFFAOYSA-N
M.W : 183.19 Pubchem ID :135423614
Synonyms :

Safety of [ 6324-72-7 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 6324-72-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6324-72-7 ]

[ 6324-72-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 6324-72-7 ]
  • [ 51012-64-7 ]
  • [ 1595278-58-2 ]
YieldReaction ConditionsOperation in experiment
46.6% With sodium hydroxide; In water; at 20℃; for 1h; General procedure: In a round bottom flask equipped with a stir bar was dissolved 2-amino-6-hydroxy-8-mercaptopurine (1-2 mmol, 1.0 equiv) in aqueous sodium hydroxide (0.4 N, 10 mL) and corresponding phenyl substituted 2-bromoacetophenones (1.25-2.5 mmol,1.25 equiv) dissolved in EtOH (2 mL) was added. The mixtures were stirred for 1 h at room temperature before the solution was neutralized by drop wise addition of HCl (1 N) to yield aprecipitate. The precipitate was collected via vacuum filtration,washed with diethyl ether and verified to be pure via LC-MS and1H NMR.
  • 2
  • [ 40299-87-4 ]
  • [ 6324-72-7 ]
  • [ 486408-79-1 ]
YieldReaction ConditionsOperation in experiment
43% With sodium hydroxide; In water; at 20℃; for 1h; General procedure: In a round bottom flask equipped with a stir bar was dissolved 2-amino-6-hydroxy-8-mercaptopurine (1-2 mmol, 1.0 equiv) in aqueous sodium hydroxide (0.4 N, 10 mL) and corresponding phenyl substituted 2-bromoacetophenones (1.25-2.5 mmol,1.25 equiv) dissolved in EtOH (2 mL) was added. The mixtures were stirred for 1 h at room temperature before the solution was neutralized by drop wise addition of HCl (1 N) to yield aprecipitate. The precipitate was collected via vacuum filtration,washed with diethyl ether and verified to be pure via LC-MS and1H NMR.
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