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Chemical Structure| 63024-77-1 Chemical Structure| 63024-77-1

Structure of 63024-77-1

Chemical Structure| 63024-77-1

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CAS No.: 63024-77-1

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Product Details of [ 63024-77-1 ]

CAS No. :63024-77-1
Formula : C8H6Cl2O
M.W : 189.04
SMILES Code : O=C(Cl)C1=CC=CC(CCl)=C1
MDL No. :MFCD00000682
InChI Key :YCAIYRWHKSJKEB-UHFFFAOYSA-N
Pubchem ID :2733324

Safety of [ 63024-77-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P280-P305+P351+P338-P310
Class:8
UN#:3265
Packing Group:Ⅱ

Application In Synthesis of [ 63024-77-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 63024-77-1 ]

[ 63024-77-1 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 64-17-5 ]
  • [ 63024-77-1 ]
  • [ 54589-54-7 ]
  • 2
  • [ 63024-77-1 ]
  • [ 20191-74-6 ]
  • [ 263270-83-3 ]
  • [ 263270-88-8 ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In dichloromethane; The N-(5-amino-2-ethylphenyl)-3-(4-methylpiperazin-1-ylmethyl)benzamide used as a starting material was prepared as follows: 3-Chloromethylbenzoyl chloride (11.93 g) was added to a stirred mixture of <strong>[20191-74-6]2-ethyl-5-nitroaniline</strong> (10 g), triethylamine (17.3 ml) and methylene chloride (283 ml) and the resultant mixture was stirred at ambient temperature for 16 hours. The mixture was evaporated. Methylene chloride was added to the residue and the resultant precipitate was isolated and washed in turn with 1N aqueous hydrochloric acid, a saturated aqueous sodium bicarbonate solution and diethyl ether. There was thus obtained 3-chloromethyl-N-(2-ethyl-5-nitrophenyl)benzamide (11.14 g); NMR Spectrum: (DMSOd6) 2.77 (m, 2H), 4.05 (s, 2H), 7.5-7.6 (m, 2H), 7.65-7.7 (m, 1H), 7.95-8.0 (m, 1H), 8.05-8.1 (m, 2H), 8.25 (s, 1H), 10.26 (s, 1H).
  • 3
  • [ 63024-77-1 ]
  • [ 22838-46-6 ]
  • [ 207853-12-1 ]
YieldReaction ConditionsOperation in experiment
100% With triethylamine; In water; N,N-dimethyl-formamide; (i) A solution of 3-chloromethyl benzoyl chloride (0.189 g) in DMF (2 ml) was added to a mixture of <strong>[22838-46-6]methyl 3-amino-3-phenylpropionate hydrochloride</strong> (0.215 g) and triethylamine (0.35 ml) in DMF (15 ml) with stirring at room temperature. After 3 hours, water (50 ml) was added and the mixture was extracted with dichloromethane. The organic layer was dried (MgSO4) and evaporated to give an oil which solidified under high vacuum to give methyl 3-(3-chloromethyl)benzamido-3-phenylpropionate in 100% yield; NMR (CDCl3) delta 7.72-8.7(10H, complex), 5.62(1H,m), 4.6(2H,s), 3.66(3H,s), 3.0(2H,m).
 

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