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[ CAS No. 63024-77-1 ] {[proInfo.proName]}

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Chemical Structure| 63024-77-1
Chemical Structure| 63024-77-1
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Product Details of [ 63024-77-1 ]

CAS No. :63024-77-1 MDL No. :MFCD00000682
Formula : C8H6Cl2O Boiling Point : No data available
Linear Structure Formula :- InChI Key :YCAIYRWHKSJKEB-UHFFFAOYSA-N
M.W : 189.04 Pubchem ID :2733324
Synonyms :

Safety of [ 63024-77-1 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:3265
Hazard Statements:H314 Packing Group:Ⅱ
GHS Pictogram:

Application In Synthesis of [ 63024-77-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 63024-77-1 ]

[ 63024-77-1 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 64-17-5 ]
  • [ 63024-77-1 ]
  • [ 54589-54-7 ]
  • 2
  • [ 63024-77-1 ]
  • [ 20191-74-6 ]
  • [ 263270-83-3 ]
  • [ 263270-88-8 ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In dichloromethane; The N-(5-amino-2-ethylphenyl)-3-(4-methylpiperazin-1-ylmethyl)benzamide used as a starting material was prepared as follows: 3-Chloromethylbenzoyl chloride (11.93 g) was added to a stirred mixture of <strong>[20191-74-6]2-ethyl-5-nitroaniline</strong> (10 g), triethylamine (17.3 ml) and methylene chloride (283 ml) and the resultant mixture was stirred at ambient temperature for 16 hours. The mixture was evaporated. Methylene chloride was added to the residue and the resultant precipitate was isolated and washed in turn with 1N aqueous hydrochloric acid, a saturated aqueous sodium bicarbonate solution and diethyl ether. There was thus obtained 3-chloromethyl-N-(2-ethyl-5-nitrophenyl)benzamide (11.14 g); NMR Spectrum: (DMSOd6) 2.77 (m, 2H), 4.05 (s, 2H), 7.5-7.6 (m, 2H), 7.65-7.7 (m, 1H), 7.95-8.0 (m, 1H), 8.05-8.1 (m, 2H), 8.25 (s, 1H), 10.26 (s, 1H).
  • 3
  • [ 63024-77-1 ]
  • [ 22838-46-6 ]
  • [ 207853-12-1 ]
YieldReaction ConditionsOperation in experiment
100% With triethylamine; In water; N,N-dimethyl-formamide; (i) A solution of 3-chloromethyl benzoyl chloride (0.189 g) in DMF (2 ml) was added to a mixture of <strong>[22838-46-6]methyl 3-amino-3-phenylpropionate hydrochloride</strong> (0.215 g) and triethylamine (0.35 ml) in DMF (15 ml) with stirring at room temperature. After 3 hours, water (50 ml) was added and the mixture was extracted with dichloromethane. The organic layer was dried (MgSO4) and evaporated to give an oil which solidified under high vacuum to give methyl 3-(3-chloromethyl)benzamido-3-phenylpropionate in 100% yield; NMR (CDCl3) delta 7.72-8.7(10H, complex), 5.62(1H,m), 4.6(2H,s), 3.66(3H,s), 3.0(2H,m).
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Technical Information

? Acyl Group Substitution ? Alkyl Halide Occurrence ? Baeyer-Villiger Oxidation ? Barbier Coupling Reaction ? Baylis-Hillman Reaction ? Benzylic Oxidation ? Birch Reduction ? Blanc Chloromethylation ? Bucherer-Bergs Reaction ? Catalytic Hydrogenation ? Clemmensen Reduction ? Complex Metal Hydride Reductions ? Corey-Bakshi-Shibata (CBS) Reduction ? Corey-Chaykovsky Reaction ? Fischer Indole Synthesis ? Friedel-Crafts Reaction ? General Reactivity ? Grignard Reaction ? Henry Nitroaldol Reaction ? Hiyama Cross-Coupling Reaction ? Horner-Wadsworth-Emmons Reaction ? Hydride Reductions ? Hydrogenolysis of Benzyl Ether ? Kinetics of Alkyl Halides ? Kumada Cross-Coupling Reaction ? Lawesson's Reagent ? Leuckart-Wallach Reaction ? McMurry Coupling ? Meerwein-Ponndorf-Verley Reduction ? Passerini Reaction ? Paternò-Büchi Reaction ? Petasis Reaction ? Peterson Olefination ? Pictet-Spengler Tetrahydroisoquinoline Synthesis ? Preparation of Aldehydes and Ketones ? Preparation of Alkylbenzene ? Preparation of Amines ? Prins Reaction ? Reactions of Aldehydes and Ketones ? Reactions of Alkyl Halides with Reducing Metals ? Reactions of Amines ? Reactions of Benzene and Substituted Benzenes ? Reformatsky Reaction ? Robinson Annulation ? Rosenmund Reduction ? Schlosser Modification of the Wittig Reaction ? Schmidt Reaction ? Specialized Acylation Reagents-Ketenes ? Stille Coupling ? Stobbe Condensation ? Substitution and Elimination Reactions of Alkyl Halides ? Suzuki Coupling ? Tebbe Olefination ? Ugi Reaction ? Vilsmeier-Haack Reaction ? Wittig Reaction ? Wolff-Kishner Reduction
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