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[ CAS No. 627-82-7 ] {[proInfo.proName]}

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Chemical Structure| 627-82-7
Chemical Structure| 627-82-7
Structure of 627-82-7 * Storage: {[proInfo.prStorage]}

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Product Details of [ 627-82-7 ]

CAS No. :627-82-7 MDL No. :MFCD00049316
Formula : C6H14O5 Boiling Point : -
Linear Structure Formula :O(CH2CH(OH)CH2OH)2 InChI Key :GPLRAVKSCUXZTP-UHFFFAOYSA-N
M.W : 166.17 Pubchem ID :42953
Synonyms :

Safety of [ 627-82-7 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340+P312-P305+P351+P338-P332+P313-P337+P313-P403+P233-P405-P501 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 627-82-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 627-82-7 ]

[ 627-82-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 56-81-5 ]
  • [ 5464-28-8 ]
  • [ 4740-78-7 ]
  • [ 79-14-1 ]
  • [ 623-50-7 ]
  • [ 627-82-7 ]
  • [ 556-52-5 ]
  • [ 116-09-6 ]
  • [ 107-02-8 ]
YieldReaction ConditionsOperation in experiment
62% With pretreated aluminium vanadium phosphate; In water; at 280℃; under 760.051 Torr;Catalytic behavior; Activation energy; The glycerol transformation was carried out in a continuous-flow fixed-bed reactor under atmospheric pressure, as previouslydescribed [23]. The reactor was made of stainless-steel tubing(7 mm internal diameter and 190 mm long), placed in a tubularelectric furnace. The temperature was monitored by a thermocou-ple located in the catalyst bed. The analysis of the feed and reactionproducts was carried out on-line using a multicolumn gas chro-matograph (GC) equipped with both flame ionization (FID) andthermal conductivity (TCD) detectors in parallel. The compoundswere separated in a capillary column, DB-1 (100% methylpolysilox-ane, 60 m x 0,25 mm x 0,25 m).The catalyst (100 mg) was pretreated at the reaction tempera-ture during 2 h in a N2flow (75 mL/min). A 36 wt% glycerol (99.5%,Sigma-Aldrich) aqueous solution was fed at 0.6 mL/h (0.69 mol/sof glycerol). In general, each catalytic test was conducted at least for3 h at different temperatures (220C, 250C and 280C). The reac-tion products were identified by chromatographic patterns and/or agas chromatograph-mass spectrometer (GC-MS) (VARIAN CP 3800,QUADRUPOLE MS 1200) also equipped with a capillary column DB-1. A blank test showed the absence of homogeneous reactions andthe reactor inactivity in the absence of a catalyst.
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