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Chemical Structure| 623-33-6 Chemical Structure| 623-33-6
Chemical Structure| 623-33-6

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CAS No.: 623-33-6

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Glycine Ethyl Ester HCl is used as an intermediate in the preparation of pesticides such as pyrethroid insecticides, pharmaceuticals like isoprothiolane, and other compounds such as pyrethric acid, dichloropyrethric acid, and tetrazole acetic acid. It is also used in biochemical research and formulations.

Synonyms: Glycine ethyl ester monohydrochloride

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Product Citations

Product Citations

Robert Kaw?cki ;

Abstract: N-Sulfenylimines (sulfenimines, thiooximes, N-alkylidenesulfenamides) were efficiently synthesized through the reaction of primary amines and disulfides with NBS or bromine. This reaction can be carried out in an open flask at room temperature without the need for any transition-metal-containing additives. The use of thiols instead of disulfides gave similar results. A wide range of amines were reacted with aryl and alkyldisulfides, resulting in the formation of sulfenimines in a yield of 44–99%.

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Product Details of [ 623-33-6 ]

CAS No. :623-33-6
Formula : C4H10ClNO2
M.W : 139.58
SMILES Code : O=C(OCC)CN.[H]Cl
Synonyms :
Glycine ethyl ester monohydrochloride
MDL No. :MFCD00012871
InChI Key :TXTWXQXDMWILOF-UHFFFAOYSA-N
Pubchem ID :2723640

Safety of [ 623-33-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis [ 623-33-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 623-33-6 ]
  • Downstream synthetic route of [ 623-33-6 ]

[ 623-33-6 ] Synthesis Path-Upstream   1~3

  • 1
  • [ 623-33-6 ]
  • [ 4755-77-5 ]
  • [ 29655-79-6 ]
YieldReaction ConditionsOperation in experiment
51% With triethylamine In dichloromethane Example 2 Ii; Compound 4 was prepared according to the Ref: J. Hetero. Chem. 1995, 32, 1693-1702. Then, it was reduced by NaBH4ZLiCl in ethanol solution. Further oxidation by Dess-Martin reagent gave the desired aldehyde 6 in 25 percent overall two-step yield.
References: [1] Synthetic Communications, 2000, vol. 30, # 17, p. 3171 - 3180.
[2] Patent: WO2007/124546, 2007, A1, . Location in patent: Page/Page column 63.
[3] Chemische Berichte, 1897, vol. 30, p. 590.
[4] Journal of the American Chemical Society, 1997, vol. 119, # 1, p. 86 - 93.
[5] Organic Process Research and Development, 2004, vol. 8, # 2, p. 192 - 200.
  • 2
  • [ 623-33-6 ]
  • [ 95-92-1 ]
  • [ 29655-79-6 ]
References: [1] Journal of Heterocyclic Chemistry, 1995, vol. 32, # 6, p. 1693 - 1702.
  • 3
  • [ 623-33-6 ]
  • [ 157115-85-0 ]
References: [1] European Journal of Medicinal Chemistry, 1996, vol. 31, # 2, p. 151 - 157.
 

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