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Chemical Structure| 61873-93-6 Chemical Structure| 61873-93-6
Chemical Structure| 61873-93-6

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CAS No.: 61873-93-6

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Product Details of [ 61873-93-6 ]

CAS No. :61873-93-6
Formula : C9H9NO5
M.W : 211.17
SMILES Code : O=C(OC)CC1=CC=C(O)C([N+]([O-])=O)=C1
MDL No. :MFCD04125034
Boiling Point : No data available
InChI Key :SPCRIUSIYZYZKN-UHFFFAOYSA-N
Pubchem ID :1473109

Safety of [ 61873-93-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 61873-93-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 61873-93-6 ]

[ 61873-93-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 61873-93-6 ]
  • [ 74-88-4 ]
  • [ 34837-88-2 ]
YieldReaction ConditionsOperation in experiment
96% With potassium carbonate; at 20℃; N-((4-chloro-2-methylphenyl)(phenyl)methyl)-2-methyl-2-(2-(2-methylpyridin-3- yl)benzo[a) methyl 2-(4-methoxy-3-nitrophenyl)acetateTo a solution of methyl 2-(4-hydroxy-3-nitrophenyl)acetate (4.87 g, 23.1 mmol) at rt was added K2CO3 (8 g, 58 mmol), followed by slow addition of CH3I (6.6 g, 46.5 mmol). The reaction mixture was stirred at rt overnight. The reaction mixture was then poured into ice-water (100 mL) and extracted with CH2CI2 (3 x 300 mL). The combined organic layers were washed with brine, dried over Na2S04, filtered, and concentrated to afford the title compound (5 g, 96%) as a yellow solid. LCMS-P1 : 226.0 [M+H]+; Rt: 1.438 min.
 

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