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[ CAS No. 6049-54-3 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 6049-54-3
Chemical Structure| 6049-54-3
Structure of 6049-54-3 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 6049-54-3 ]

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Product Details of [ 6049-54-3 ]

CAS No. :6049-54-3 MDL No. :MFCD00181810
Formula : C9H11NO3 Boiling Point : No data available
Linear Structure Formula :- InChI Key :-
M.W : 181.19 Pubchem ID :-
Synonyms :
Chemical Name :3-Amino-3-(4-hydroxyphenyl)propanoic Acid

Safety of [ 6049-54-3 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 6049-54-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6049-54-3 ]

[ 6049-54-3 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 7400-08-0 ]
  • [ 6049-54-3 ]
  • 2
  • methyl p-hydroxycinnamate [ No CAS ]
  • [ 6049-54-3 ]
  • 3
  • [ 5678-45-5 ]
  • [ 6049-54-3 ]
  • 4
  • [ 141-82-2 ]
  • [ 123-08-0 ]
  • [ 6049-54-3 ]
  • [ 17449-03-5 ]
  • 5
  • [ 141-82-2 ]
  • [ 123-08-0 ]
  • [ 6049-54-3 ]
YieldReaction ConditionsOperation in experiment
70% With ammonium acetate; In butan-1-ol;Reflux; General procedure: A mixture of appropriate aldehyde 2.40 g (1-15), 2.44 g ofmalonic acid and 3.54 g of ammonium acetate (1:1.1:2.3), in 200mLof the 1-butanol was refluxed for 1.5-2 h until the evolution of CO2ceased. The precipitate formed was filtered and washed withboiling 1-butanol (2 x 50 mL), boiling ethanol (2 x 50 mL) and100mL of water. Precipitates were dried at 80-100 C for 8-10 h.Purity of product was checked by TLC, and yield obtained about65-80% in each reaction.
65% To a 2 liter three-mouth flask in of hydroxy benzaldehyde (100 g, 0 . 82 μM), ammonia acetate (126 g, 1 . 64 μM) and volume than 97.5% of ethanol (1.2 L). 40 C when stirring 30 minutes; then adding malonic acid (170 g, 1 . 64 μM), heating reflux for 60 hours. After cooling to room temperature, filtering and separating the white solid, for the volume ratio of 1:1 of ethanol and water mixed solution (100 ml) washing, vacuum drying to obtain a white solid, compound 1 (88.8 g, 0 . 53 μM, 65%).
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