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CAS No. : | 589-18-4 | MDL No. : | MFCD00004664 |
Formula : | C8H10O | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | KMTDMTZBNYGUNX-UHFFFAOYSA-N |
M.W : | 122.16 | Pubchem ID : | 11505 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
61% | With potassium carbonate; In N,N-dimethyl-formamide; at 80℃; for 2h; | A typical synthetic procedure is as follows. 1,7-dibromo perylene diimide (1, 77 mg, 0.1 mmol) was dissolved into 5 mL of dimethylformamide (DMF). To which alkyl alcohol (R-OH, 0.5 mmol) and potassium carbonate (K2CO3, 70 mg, 0.5 mmol) were added. The resulted mixture was then allowed reacted under 80C for 1-4 hours. The reaction mixture was then powered into 15 mL water and the red solid was then re-dissolved in 20 mL dichloromethane (DCM) and washed with 1N hydrochloric acid and then water each for 3 times. Then, DCM layer was dried over Na2SO4. After removal of DCM, the residue was applied to chromatography with CH2Cl2/ethyl acetate (100:0-100:2) as eluents to afford the desired products 4. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
91% | With 4-Methylbenzyl bromide; at 130℃; for 12h;Green chemistry; | <strong>[4214-79-3]2-hydroxy-5-chloropyridine</strong> (0.259 g, 2 mmol), 4-methylbenzyl alcohol(2.4 mmol, 1.2 equiv.) And 4-methylbenzyl bromide (0.0559 ml, 20 molpercent)were added successively to a tubular reactor,, Sealed directly in air, and thenheated to 130 ° C for 12 h undersolvent-freeconditions.After the TLC monitoring reaction was complete, the product was purified by column chromatography and the yield was91percent. |
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