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CAS No. : | 51871-62-6 | MDL No. : | MFCD01076271 |
Formula : | C15H21NO4 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | ACKWQHCPHJQANL-LBPRGKRZSA-N |
M.W : | 279.33 | Pubchem ID : | 2761538 |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | |
Hazard Statements: | H302 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With trifluoroacetic acid; In dichloromethane; at 20℃; for 2h; | [00293] (S)-3-Amino-4-phenylbutanoic acid: (S)-3-(tert-Butoxycarbonyl)-4- phenylbutanoic acid (Ig, 3.58 mmol) was dissolved in 20 mL DCM and 6 mL TFA was added at room temperature. The mixture was stirred for 2 hours and the mixture was azeotroped 3 times with 25 mL toluene (each). The product thus obtained was used without further purification in the next step. LCMS (API-ES) m/z (%): 179.1 (100%, M++H). |
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