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Chemical Structure| 516-06-3 Chemical Structure| 516-06-3
Chemical Structure| 516-06-3

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CAS No.: 516-06-3

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H-DL-Val-OH is a valine derivative that plays a role in protein synthesis, energy metabolism, and muscle repair. This compound can be used in metabolic regulation, sports nutrition, and protein engineering research.

Synonyms: DL-Valine

4.5 *For Research Use Only !

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Product Details of H-DL-Val-OH

CAS No. :516-06-3
Formula : C5H11NO2
M.W : 117.15
SMILES Code : NC(C(C)C)C(O)=O
Synonyms :
DL-Valine
MDL No. :MFCD00004267

Safety of H-DL-Val-OH

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P301+P312-P302+P352-P304+P340-P305+P351+P338

Application In Synthesis of H-DL-Val-OH

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 516-06-3 ]

[ 516-06-3 ] Synthesis Path-Downstream   1~12

  • 1
  • [ 540-88-5 ]
  • [ 516-06-3 ]
  • [ 6070-59-3 ]
YieldReaction ConditionsOperation in experiment
With perchloric acid; at 20℃; for 36h; Step 1: tert-butyl 2-amino-3-methylbutanoateTo a stirred solution of DL- valine (25 g, 0.213 mol) in tert-butyl acetate (250 mL) at 0C, was added HCI04 (64.2 g, 0.320 mol) portionwise. The reaction mixture was stirred for 36 h at RT. It was diluted with water and extracted in ethyl acetate (500 mL). The organic layer was washed with a 10% sodium bicarbonate solution (2x150 mL), dried over Na2S04 and concentrated, affording of the title compound as brown liquid. 1H NMR (DMSO-d6, 400 MHz) δ 7.31 (brs, 2H), 3.62(d, J = 4.4 Hz, 1 H), 1 .98 (d, J = 1.7 Hz, 1 H), 1.44(s, 9H), 0.95 (m, 6H).
  • 2
  • [ 1184-90-3 ]
  • [ 516-06-3 ]
  • [ 35404-64-9 ]
  • 3
  • [ 516-06-3 ]
  • [ 169556-48-3 ]
  • 4
  • [ 516-06-3 ]
  • [ 59804-37-4 ]
  • manganese(ll) chloride [ No CAS ]
  • [Mn(H2Ten)(Val)(H2O)2]Cl [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; water; for 2h;Reflux; General procedure: The metal chlorides of Fe(III), Co(II), Ni(II), Cu(II),Mn(II), Cr(III) andZn(II) solutions (1 mmol) in bidistilled water (25 mL) were added to25 mL ethanol solution of H2Ten (0.337 g, 1mmol) followed by additionof 25 mL of 1 mmol Val (0.117 g in bidistilled water) in the molar ratio1:1:1 (metal salt: H2Ten: Val) in total volume 75 mL mixture. Theresulting mixture was stirred under reflux for 2 h whereupon the complexes precipitated. They were removed by filtration, washed withhot ethanol followed by diethylether and dried in vacuum desiccatorsover anhydrous calcium chloride
  • 5
  • [ 7732-18-5 ]
  • [ 516-06-3 ]
  • [ 59804-37-4 ]
  • [ 7646-85-7 ]
  • [Zn(H2Ten)(Val)(H2O)2]Cl [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; for 2h;Reflux; General procedure: The metal chlorides of Fe(III), Co(II), Ni(II), Cu(II),Mn(II), Cr(III) andZn(II) solutions (1 mmol) in bidistilled water (25 mL) were added to25 mL ethanol solution of H2Ten (0.337 g, 1mmol) followed by additionof 25 mL of 1 mmol Val (0.117 g in bidistilled water) in the molar ratio1:1:1 (metal salt: H2Ten: Val) in total volume 75 mL mixture. Theresulting mixture was stirred under reflux for 2 h whereupon the complexes precipitated. They were removed by filtration, washed withhot ethanol followed by diethylether and dried in vacuum desiccatorsover anhydrous calcium chloride
  • 6
  • iron(III) chloride hexahydrate [ No CAS ]
  • [ 516-06-3 ]
  • [ 59804-37-4 ]
  • [Fe(H2Ten)(Val)(H2O)2]Cl2*2H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; water; for 2h;Reflux; General procedure: The metal chlorides of Fe(III), Co(II), Ni(II), Cu(II),Mn(II), Cr(III) andZn(II) solutions (1 mmol) in bidistilled water (25 mL) were added to25 mL ethanol solution of H2Ten (0.337 g, 1mmol) followed by additionof 25 mL of 1 mmol Val (0.117 g in bidistilled water) in the molar ratio1:1:1 (metal salt: H2Ten: Val) in total volume 75 mL mixture. Theresulting mixture was stirred under reflux for 2 h whereupon the complexes precipitated. They were removed by filtration, washed withhot ethanol followed by diethylether and dried in vacuum desiccatorsover anhydrous calcium chloride
  • 7
  • chromium(III) chloride hexahydrate [ No CAS ]
  • [ 516-06-3 ]
  • [ 59804-37-4 ]
  • [Cr(H2Ten)(Val)(H2O)2]Cl2*4H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; water; for 2h;Reflux; General procedure: The metal chlorides of Fe(III), Co(II), Ni(II), Cu(II),Mn(II), Cr(III) andZn(II) solutions (1 mmol) in bidistilled water (25 mL) were added to25 mL ethanol solution of H2Ten (0.337 g, 1mmol) followed by additionof 25 mL of 1 mmol Val (0.117 g in bidistilled water) in the molar ratio1:1:1 (metal salt: H2Ten: Val) in total volume 75 mL mixture. Theresulting mixture was stirred under reflux for 2 h whereupon the complexes precipitated. They were removed by filtration, washed withhot ethanol followed by diethylether and dried in vacuum desiccatorsover anhydrous calcium chloride
  • 8
  • cobalt(II) chloride hexahydrate [ No CAS ]
  • [ 516-06-3 ]
  • [ 59804-37-4 ]
  • [Co(H2Ten)(Val)(H2O)2]Cl*H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; water; for 2h;Reflux; General procedure: The metal chlorides of Fe(III), Co(II), Ni(II), Cu(II),Mn(II), Cr(III) andZn(II) solutions (1 mmol) in bidistilled water (25 mL) were added to25 mL ethanol solution of H2Ten (0.337 g, 1mmol) followed by additionof 25 mL of 1 mmol Val (0.117 g in bidistilled water) in the molar ratio1:1:1 (metal salt: H2Ten: Val) in total volume 75 mL mixture. Theresulting mixture was stirred under reflux for 2 h whereupon the complexes precipitated. They were removed by filtration, washed withhot ethanol followed by diethylether and dried in vacuum desiccatorsover anhydrous calcium chloride
  • 9
  • nickel(II) chloride hexahydrate [ No CAS ]
  • [ 516-06-3 ]
  • [ 59804-37-4 ]
  • [Ni(H2Ten)(Val)(H2O)2]Cl*H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; water; for 2h;Reflux; General procedure: The metal chlorides of Fe(III), Co(II), Ni(II), Cu(II),Mn(II), Cr(III) andZn(II) solutions (1 mmol) in bidistilled water (25 mL) were added to25 mL ethanol solution of H2Ten (0.337 g, 1mmol) followed by additionof 25 mL of 1 mmol Val (0.117 g in bidistilled water) in the molar ratio1:1:1 (metal salt: H2Ten: Val) in total volume 75 mL mixture. Theresulting mixture was stirred under reflux for 2 h whereupon the complexes precipitated. They were removed by filtration, washed withhot ethanol followed by diethylether and dried in vacuum desiccatorsover anhydrous calcium chloride
  • 10
  • copper(II) chloride hexahydrate [ No CAS ]
  • [ 516-06-3 ]
  • [ 59804-37-4 ]
  • [Cu(H2Ten)(Val)(H2O)2]Cl*H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; water; for 2h;Reflux; General procedure: The metal chlorides of Fe(III), Co(II), Ni(II), Cu(II),Mn(II), Cr(III) andZn(II) solutions (1 mmol) in bidistilled water (25 mL) were added to25 mL ethanol solution of H2Ten (0.337 g, 1mmol) followed by additionof 25 mL of 1 mmol Val (0.117 g in bidistilled water) in the molar ratio1:1:1 (metal salt: H2Ten: Val) in total volume 75 mL mixture. Theresulting mixture was stirred under reflux for 2 h whereupon the complexes precipitated. They were removed by filtration, washed withhot ethanol followed by diethylether and dried in vacuum desiccatorsover anhydrous calcium chloride
  • 11
  • [ 516-06-3 ]
  • [ 16935-34-5 ]
 

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