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CAS No. : | 499-75-2 | MDL No. : | MFCD00002236 |
Formula : | C10H14O | Boiling Point : | - |
Linear Structure Formula : | OHC6H3(CH3)CH(CH3)2 | InChI Key : | RECUKUPTGUEGMW-UHFFFAOYSA-N |
M.W : | 150.22 | Pubchem ID : | 10364 |
Synonyms : |
Cymophenol;p-Cymen-2-ol;Karvakrol;BRN-1860514;Antioxine;NSC 6188;Isopropyl o-cresol
|
Chemical Name : | 5-Isopropyl-2-methylphenol |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H317-H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
General procedure: Suitably protected compounds (16-20, 23-26,and 28) (5.1 mmol) were dissolved in DMF (2 mL) and DCM (10 mL), and then added with DCC (5.1 mmol). After 1 h under stirring at room temperature, the reaction mixture was added with DMAP (0.16 mmol) and carvacrol (5.1 mmol) and stirred overnight at room temperature. After reduced pressure filtration, the solvent was evaporated and the residue was extracted with AcOEt/NaCl ss. The organic layer was dried over anhydrous Na2SO4 and evaporated under vacuum. Chromatographic purification with DCM/AcOEt 1:1 as eluant provided the desired compounds in good yields (2-7, 9-10, 21, and 27). |