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[ CAS No. 4072-67-7 ] {[proInfo.proName]}

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Chemical Structure| 4072-67-7
Chemical Structure| 4072-67-7
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Product Details of [ 4072-67-7 ]

CAS No. :4072-67-7 MDL No. :MFCD00017877
Formula : C16H12Br2O2 Boiling Point : -
Linear Structure Formula :- InChI Key :RTSLQVZQORGDQQ-UHFFFAOYSA-N
M.W : 396.07 Pubchem ID :77689
Synonyms :

Safety of [ 4072-67-7 ]

Signal Word:Danger Class:8
Precautionary Statements:P501-P260-P270-P264-P280-P303+P361+P353-P301+P330+P331-P363-P301+P312+P330-P304+P340+P310-P305+P351+P338+P310-P405 UN#:3261
Hazard Statements:H302-H314 Packing Group:Ⅱ
GHS Pictogram:

Application In Synthesis of [ 4072-67-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4072-67-7 ]

[ 4072-67-7 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 5344-27-4 ]
  • [ 4072-67-7 ]
  • 4,4'-bis-[4-(2-hydroxy-ethyl)-pyridinioacetyl]-biphenyl; dibromide [ No CAS ]
  • 2
  • [ 3616-56-6 ]
  • [ 4072-67-7 ]
  • [ 13717-24-3 ]
  • 3
  • [ 186581-53-3 ]
  • [ 4072-67-7 ]
  • [ 792-74-5 ]
  • 4
  • [ 15761-39-4 ]
  • [ 4072-67-7 ]
  • [ 1007882-23-6 ]
YieldReaction ConditionsOperation in experiment
60.0 g 4,4?-Bis(2-bromoacetyl)biphenyl bOg was added to methylene dichloride (l000ml) andstirred to get solution. Boc-L-Proline (120g) was added to it. Diisopropylethylamine68.5g was added to the reaction mass at 15-25C. The reaction mass was stirred for about4 to 5h. The reaction mass was quenched by adding water. The aqueous layer was separated and organic layer was washed with aqueous acetic acid solution (Conc HC1 also can be used instead of acetic acid) till pH of aqueous layer was between 4-6. Theorganic layer was washed with water and distilled under vacuum to get a residue. The residue was dissolved in toluene and toluene solution was used further. Ammonium acetate 390g was added to the toluene solution and the reaction mass was stirred. The reaction mass heated to 95-105C and maintained till completion of reaction. After completion of the reaction, the reaction mass was cooled to 50-60C, methanol wasadded and the reaction mass cooled to 20-30C and stirred for 2 to 3 hours. The solid was filtered and washed with toluene. Purity of crude:- 93.92%.Crude wet cake was stirred in mixture of toluene, methanol and acetic acid and the reaction mass was heated to 60- 70C, water was added to reaction mass at 60-70C and the reaction mass cooled to 20-30C and stirred. The solid obtained was filtered and washed with toluene and then withwater. Wet solid was dried. Purity - 97.04%. The above purification was repeated to obtain 60.Og of the title compound in a purity of 98.97%.
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Technical Information

? Alkyl Halide Occurrence ? Baeyer-Villiger Oxidation ? Barbier Coupling Reaction ? Baylis-Hillman Reaction ? Benzylic Oxidation ? Birch Reduction ? Blanc Chloromethylation ? Bucherer-Bergs Reaction ? Clemmensen Reduction ? Corey-Bakshi-Shibata (CBS) Reduction ? Corey-Chaykovsky Reaction ? Fischer Indole Synthesis ? Friedel-Crafts Reaction ? General Reactivity ? Grignard Reaction ? Henry Nitroaldol Reaction ? Hiyama Cross-Coupling Reaction ? Horner-Wadsworth-Emmons Reaction ? Hydride Reductions ? Hydrogenolysis of Benzyl Ether ? Kinetics of Alkyl Halides ? Kumada Cross-Coupling Reaction ? Lawesson's Reagent ? Leuckart-Wallach Reaction ? McMurry Coupling ? Meerwein-Ponndorf-Verley Reduction ? Passerini Reaction ? Paternò-Büchi Reaction ? Petasis Reaction ? Peterson Olefination ? Pictet-Spengler Tetrahydroisoquinoline Synthesis ? Preparation of Aldehydes and Ketones ? Preparation of Alkylbenzene ? Preparation of Amines ? Prins Reaction ? Reactions of Aldehydes and Ketones ? Reactions of Alkyl Halides with Reducing Metals ? Reactions of Amines ? Reactions of Benzene and Substituted Benzenes ? Reactions of Dihalides ? Reformatsky Reaction ? Robinson Annulation ? Schlosser Modification of the Wittig Reaction ? Schmidt Reaction ? Specialized Acylation Reagents-Ketenes ? Stille Coupling ? Stobbe Condensation ? Substitution and Elimination Reactions of Alkyl Halides ? Suzuki Coupling ? Tebbe Olefination ? Ugi Reaction ? Vilsmeier-Haack Reaction ? Wittig Reaction ? Wolff-Kishner Reduction
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