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Chemical Structure| 402-14-2 Chemical Structure| 402-14-2
Chemical Structure| 402-14-2

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CAS No.: 402-14-2

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Product Details of [ 402-14-2 ]

CAS No. :402-14-2
Formula : C7H5F3N2O2
M.W : 206.12
SMILES Code : NC1=CC(C(F)(F)F)=CC=C1[N+]([O-])=O
MDL No. :MFCD00042447
InChI Key :AUTLVHYEAAAKNM-UHFFFAOYSA-N
Pubchem ID :223100

Safety of [ 402-14-2 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302+H312-H315-H319-H331-H335
Precautionary Statements:P261-P280-P305+P351+P338-P311
Class:6.1
UN#:2811
Packing Group:

Application In Synthesis of [ 402-14-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 402-14-2 ]

[ 402-14-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 402-14-2 ]
  • [ 683241-86-3 ]
YieldReaction ConditionsOperation in experiment
With N-Bromosuccinimide; In acetic acid; for 4.0h;Reflux; A mixture of 3-amino-4-nitrobenzotrifluoride (5.4 g, 26.2 mmol) and N-bromosuccinimide (4.59 g, 25.8 mmol) in acetic acid was heated under reflux, with stirring, for 4 h. The reaction mixture was cooled and poured into 1.5 L of water with agitation. The precipitate was suction-filtered to give a yellow solid that was further purified by silica gel column chromatography (0 to 40% ethyl acetate in hexanes) to afford the title compound as a yellow solid. LC-MS: 285.03(M-), 2.75 min (LC/MS method A)
 

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