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[ CAS No. 38565-52-5 ] {[proInfo.proName]}

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Chemical Structure| 38565-52-5
Chemical Structure| 38565-52-5
Structure of 38565-52-5 * Storage: {[proInfo.prStorage]}

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Product Details of [ 38565-52-5 ]

CAS No. :38565-52-5 MDL No. :MFCD00042356
Formula : C9H5F13O Boiling Point : No data available
Linear Structure Formula :- InChI Key :KGYUZRBIQCDOCN-UHFFFAOYSA-N
M.W : 376.11 Pubchem ID :170073
Synonyms :

Safety of [ 38565-52-5 ]

Signal Word:Danger Class:3
Precautionary Statements:P210-P264-P280-P302+P352+P332+P313+P362+P364-P305+P351+P338+P337+P313-P403+P235-P501 UN#:1993
Hazard Statements:H225-H315-H319 Packing Group:Ⅱ
GHS Pictogram:

Application In Synthesis of [ 38565-52-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 38565-52-5 ]

[ 38565-52-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 926-39-6 ]
  • [ 38565-52-5 ]
  • [ 1262880-11-4 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; In water; isopropyl alcohol; at 65℃; for 15h; 100 ml glass container was charged with 1.7 g of 20percent aqueous sodium hydroxide, 4.6 g of ion exchanged water, 6 g of isopropyl alcohol, 1.0 g (0.007 mol) of 2-aminoethyl hydrogen sulfate (Manufactured by Tokyo Kasei Kogyo Co. Ltd.), and 5.3 g (0.014 mol) of the compound (3-1) which had been synthesized by the method known in the art, and after sealing, the mixture was set on a water bath shaker to allow for the reaction to proceed at 65°C for 15 hours to obtain a compound reaction product mainly comprising the compound (1-4). Since solid precipitation and sedimentation of a transparent liquid was partly observed, upper layer was collected and filtered through a 0.45 mum filter to obtain a water/isopropyl alcohol solution containing 28percent of the reaction product mainly comprising the compound (1-4). The yield was 78percent. In the gas chromatographic analysis of the reaction solution, the conversion rate of the compound (3-1) was 96percent. To confirm the identity of the reaction product, a portion of the reaction solution was dried at 40°C for 4 hours at a reduced pressure of 10 mmHg, and the resulting solid was analyzed by NMR. 1H-NMR and 13C-NMR spectrum data for the compound (1-4) were as shown below. 1H-NMR (300 MHz, solvent: CD3OD, standard substance: hexamethyldisiloxane), sigma (ppm) : 2.0 to 2.5 (4H), 2.5 to 2.7 (4H), 2.7 to 3.0 (2H), 4.0 to 4.3(6H) 13C-NMR (300 MHz, solvent: CD3OD, standard substance: hexamethyldisiloxane), sigma (ppm): 36.6 (t), 36.8 (t), 55.1, 55.5, 63.4, 64.0, 64.8, 66.9
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