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[ CAS No. 354-37-0 ] {[proInfo.proName]}

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Chemical Structure| 354-37-0
Chemical Structure| 354-37-0
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Product Details of [ 354-37-0 ]

CAS No. :354-37-0 MDL No. :MFCD00041545
Formula : C2H3F3N2 Boiling Point : -
Linear Structure Formula :- InChI Key :NITMACBPVVUGOJ-UHFFFAOYSA-N
M.W : 112.05 Pubchem ID :2776882
Synonyms :

Safety of [ 354-37-0 ]

Signal Word:Danger Class:8
Precautionary Statements:P260-P301+P330+P331-P303+P361+P353-P305+P351+P338-P405-P501 UN#:3267
Hazard Statements:H314 Packing Group:Ⅱ
GHS Pictogram:

Application In Synthesis of [ 354-37-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 354-37-0 ]

[ 354-37-0 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 7732-18-5 ]
  • [ 354-37-0 ]
  • [ 87-13-8 ]
  • [ 343-67-9 ]
YieldReaction ConditionsOperation in experiment
50% With NaOEt In ethanol Example 33
ETHYL 2-TRIFLUOROMETHYL-4-HYDROXYPYRIMIDINE-5-CARBOXYLATE
A solution of diethyl ethoxymethylenemalonate (35.0 g, 162 mmol), trifluoroacetamidine (18 g, 162 mmol) and NaOEt (11.0 g, 162 mmol) in EtOH (200 mL) was heated at reflux for 6 h.
The reaction mixture was concentrated and H2 O (48 mL) was added.
The resulting solid was filtered, washed with Et2 O (300 mL) and H2 O (200 mL), and dried to give the title compound (21 g, 50percent yield); m.p. >220° C. (dec.); 1 H-NMR (DMSO-d6) δ 8.38, 4.16 (q, 2H), 1.25 (q, 3H).
Reference： [1] Patent: US5811428, 1998, A,
  • 2
  • [ 354-37-0 ]
  • [ 87-13-8 ]
  • [ 343-67-9 ]
Reference： [1] Journal of medicinal chemistry, 2000, vol. 43, # 21, p. 3995 - 4004
[2] Bioorganic and Medicinal Chemistry Letters, 2000, vol. 10, # 15, p. 1645 - 1648
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