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Chemical Structure| 34253-03-7 Chemical Structure| 34253-03-7
Chemical Structure| 34253-03-7

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CAS No.: 34253-03-7

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Synonyms: methyl 2-Pyrimidine Carboxylate

4.5 *For Research Use Only !

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Product Details of Methyl pyrimidine-2-carboxylate

CAS No. :34253-03-7
Formula : C6H6N2O2
M.W : 138.12
SMILES Code : O=C(C1=NC=CC=N1)OC
Synonyms :
methyl 2-Pyrimidine Carboxylate
MDL No. :MFCD03426929
InChI Key :JOQJEWAXHQDQAG-UHFFFAOYSA-N
Pubchem ID :3613871

Safety of Methyl pyrimidine-2-carboxylate

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of Methyl pyrimidine-2-carboxylate

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 34253-03-7 ]

[ 34253-03-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 34253-03-7 ]
  • [ 790667-49-1 ]
  • (2S)-tert-butyl 2-methyl-4-oxo-5-(pyrimidine-2-carbonyl)piperidine-1-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
73.47% To a mixture of (S)-tert-butyl 2-methyl -4-oxopiperidine-1-carboxylate (5 g, 23.44 mmol) in THF (40 mL) was added LiHMDS (1 M, 46.88 mL) in one portion at 0 C under N2. The reaction mixture was stirred at 0 C for 0.5 h, then methyl pyrimidine-2-carboxylate (5.50 g, 39.85 mmol) in THF (40 mL) was added into the solution at 0 C and stirred at 15 C for 4 hours. The reaction mixture was poured into aq. NH4CI (200 mL) and stirred for 1 min. The aqueous phase was extracted with ethyl acetate (200 mL/2). The organics layers were separated, washed with brine (100 mL/2). dried with anhydrous NaaSCL, fdtered and concentrated in vacuum. Purification (FCC, S1O2, Petroleum ether/Ethyl acetate=l0/l to 0: 1) afforded (2S)-tert-butyl 2-methyl-4-oxo-5-(pyrimidine-2-carbonyl)piperidine-l-carboxylate (5.5 g, 17.22 mmol, 73.47% yield) as a yellow oil. MS (ESI): mass ealed. for C16H21N3O4, 319.2; m/z found, 342.1 [M+Na]+.
  • 2
  • [ 34253-03-7 ]
  • [ 16932-45-9 ]
  • (2,6-dimethoxyphenyl)(pyrimidin-2-yl)methanone [ No CAS ]
 

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