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[ CAS No. 3383-21-9 ] {[proInfo.proName]}

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Chemical Structure| 3383-21-9
Chemical Structure| 3383-21-9
Structure of 3383-21-9 * Storage: {[proInfo.prStorage]}

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Product Details of [ 3383-21-9 ]

CAS No. :3383-21-9 MDL No. :MFCD00001647
Formula : C14H20O2 Boiling Point : -
Linear Structure Formula :O2(C(CH3)3)2C6H2 InChI Key :NOUZOVBGCDDMSX-UHFFFAOYSA-N
M.W : 220.31 Pubchem ID :76915
Synonyms :

Safety of [ 3383-21-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 3383-21-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 3383-21-9 ]

[ 3383-21-9 ] Synthesis Path-Downstream   1~6

  • 1
  • [ 3383-21-9 ]
  • [ 262373-15-9 ]
  • 1,3-di-tert-butyl-6-methyl-1,4-dihydro-1,4-ethanonaphthalene-9,10-dione [ No CAS ]
  • 1,3-di-tert-butyl-7-methyl-1,4-dihydro-1,4-ethanonaphthalene-9,10-dione [ No CAS ]
  • 2
  • [ 558478-81-2 ]
  • [ 3383-21-9 ]
  • 5-cyclopropyl-1-(3,5-di-tert-butyl-2-hydroxyphenyl)pyrrolidin-2-one [ No CAS ]
  • 3
  • [ 558478-81-2 ]
  • [ 3383-21-9 ]
  • 5,7-Ditert-butyl-1-cyclopropyl-1,2,3,3a-tetrahydrobenzo[d]pyrrolo[2,1-b]-oxazole [ No CAS ]
  • 4
  • 2,4-di-tert-butyl-6-(2-cyclopropylpyrrolidin-1-yl)phenol [ No CAS ]
  • [ 558478-81-2 ]
  • [ 3383-21-9 ]
  • 5
  • [ 3383-21-9 ]
  • [ 134855-87-1 ]
  • 4-(6,8-di-tert-butyl-2H-benzo[b][1,4]oxazin-3-yl)phenol [ No CAS ]
  • 6
  • [ 3383-21-9 ]
  • [ 134855-87-1 ]
  • C22H29NO2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
In acetonitrile; at 20℃;Inert atmosphere; General procedure: To a stirred solution of ortho-benzoquinone (0.825 mmol, 1.0equiv) in acetonitrile (4.0 mL), was added dropwise a solution ofprimary amine (0.825 mmol, 1.0 equiv) in acetonitrile (4.25 mL)over 5 min under an argon atmosphere. The deep green colouredsolution was stirred at room temperature for 2e8 h. Aftercompletion of the reaction, as indicated by TLC, the reactionmixture was cooled to 0C. To this, triethylamine (0.34 mL,2.48 mmol, 3 equiv) and iodine granules (0.419 g, 1.65 mmol, 2 eq),were added. The resulting mixture was stirred vigorously for10e60 min under argon atmosphere. Upon completion, the reac-tion mixture was diluted with water and extracted with EtOAc(3 5 mL). The combined organic layer was washed with aqueoussaturated sodium thiosulfate (1 10 mL) and brine (2 10 mL),respectively, dried over Na2SO4, ltered, and concentrated in vacuo.The crude residue was puried by silica gel column chromatog-raphy eluting with pentane:EtOAc (95:5e80:20 v:v) to afford thedesired benzo[1,4]oxazine product.
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