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CAS No. : | 3306-62-5 | MDL No. : | MFCD00007932 |
Formula : | C6H8N2O2S | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | YAZSBRQTAHVVGE-UHFFFAOYSA-N |
M.W : | 172.21 | Pubchem ID : | 72894 |
Synonyms : |
Orthanilamide;O-Sulfanilamide;Benzenesulfonamide;O-Aminobenzenesulfonamide
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
19% | With pyridine; for 12.0h; | 2-Aminobenzenesulfonamide (54 mg, 0.31 mmol) and <strong>[351003-48-0]3-chloro-2-fluoro-benzenesulfonyl chloride</strong> (47 mg, 0.21 mmol) were dissolved in pyridine (1 ml) and the reaction mixture was stirred for 12 h. The solvent was removed in vacuo and the residue was purified by HPLC to give the product (15 mg, 19%).1H NMR (400 MHz, DMSO-d6) delta ppm 9.72 (br. s., 1H), 7.90 (t, 1H), 7.78-7.86 (m, 2H), 7.73 (br. s., 2H), 7.51-7.58 (m, 1H), 7.46-7.51 (m, 1H), 7.39 (t, 1H), 7.26-7.34 (m, 1H);MS m/z M-H 363. |