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CAS No. : | 3158-26-7 | MDL No. : | MFCD00013887 |
Formula : | C9H17NO | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | DYQFCTCUULUMTQ-UHFFFAOYSA-N |
M.W : | 155.24 | Pubchem ID : | 76616 |
Synonyms : |
|
Chemical Name : | Octylisocyanate |
Signal Word: | Danger | Class: | 6.1 |
Precautionary Statements: | P210-P261-P264-P270-P271-P280-P284-P301+P312+P330-P302+P352-P304+P340+P312-P305+P351+P338-P332+P313-P337+P313-P342+P311-P370+P378-P403+P233-P403+P235-P405-P501 | UN#: | 2206 |
Hazard Statements: | H227-H302-H315-H319-H334-H335 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With lithium diisopropyl amide; | EXAMPLE 13 Preparation of N-octyl-beta-oxo-9-anthracenepropanamide The title compound, mp 70-72 C., was prepared from <strong>[784-04-3]9-acetylanthracene</strong> (5.0 g, 0.022 mol), octyl isocyanate (3.52 g, 0.022 mol), and lithium diisopropylamide (0.032 mol) using the procedure described in Example 1. Purification by flash chromatography (silica gel, 5% EtOAc/hexane) yielded 3.84 g (0.010 mol, 45.2%) of the desired product. Analysis for C25 H29 NO2: Calcd: C, 79.96; H, 7.78; N, 3.73; Found: C, 80.07; H, 7.94; N, 3.62. |