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[ CAS No. 31001-77-1 ] {[proInfo.proName]}

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Chemical Structure| 31001-77-1
Chemical Structure| 31001-77-1
Structure of 31001-77-1 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 31001-77-1 ]

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Product Details of [ 31001-77-1 ]

CAS No. :31001-77-1 MDL No. :MFCD00053923
Formula : C6H16O2SSi Boiling Point : -
Linear Structure Formula :- InChI Key :IKYAJDOSWUATPI-UHFFFAOYSA-N
M.W : 180.34 Pubchem ID :2759524
Synonyms :

Safety of [ 31001-77-1 ]

Signal Word:Danger Class:9
Precautionary Statements:P501-P273-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 UN#:3334
Hazard Statements:H315-H319-H413-H372 Packing Group:Ⅲ
GHS Pictogram:

Application In Synthesis of [ 31001-77-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 31001-77-1 ]

[ 31001-77-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 69655-76-1 ]
  • [ 31001-77-1 ]
  • C64H152O28S8Si16 [ No CAS ]
YieldReaction ConditionsOperation in experiment
Ca.100% With 2,2-dimethoxy-2-phenylacetophenone; In tetrahydrofuran; at 20℃; for 0.25h;UV-irradiation; Inert atmosphere; In a vial, OVS (0.5g, 0.79mmol), 1.0equiv (to ?Vi goups) of 3?mercaptopropylmethyldimethoxysilane (1.14g, 6.33mmol) and 2wtpercent of DMPA were dissolved in the minimal amount of anhydrous THF under the argon condition. The mixture was irradiated with stirring for 15min with UV light at room temperature. The solvent was evaporated in vacuo and then washed by distilled methanol to obtain SQ?[SiMe(OMe)2]8 as a viscous pale yellow oil (1.64g, yield ?100percent). SQ?[SiMe(OMe)2]8 can also be prepared without DMPA after 90min of irradiation. 1H NMR (300MHz, CDCl3, ppm): delta=0.13 (s, ?SiCH3, 24H), 0.72?0.76 (t, ?CH2Si(OCH3)2?, J=6.3Hz, 16H), 0.99?1.03 (t, ?SiCH2CH2S?, J=6.4Hz, 16H), 1.62?1.70 (m, ?SCH2CH2CH2?, 16H), 2.53?2.61 (m, ?CH2SCH2?, 32H), 3.52 (s, ?Si(OCH3)2?, 48H). 13C NMR (75MHz, CDCl3, ppm): delta=?5.80 (?SiCH3), 12.66 (?CH2Si(OCH3)2?), 13.03 (?SiCH2CH2), 22.95 (?SCH2CH2CH2?), 25.86 (?SiCH2CH2), 35.05 (?SCH2CH2CH2), 50.14 (?Si(OCH3)2?). 29Si NMR (60Hz, CDCl3, ppm): delta=?68.93 (?SiCH2CH2), ?1.91 (?SiMe(OMe3)2). FTIR (KBr, cm?1): 2926, 2836, 2359, 1452, 1411, 1258, 1123, 1082, 823; MS?ESI: 1007.21 [M?2OCH3]2+. Anal. Calcd for C64H152O28S8Si16: C, 37.03; H, 7.38; S, 12.36. Found: C, 36.90; H, 7.40; S, 12.39.
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