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CAS No. : | 28900-10-9 | MDL No. : | MFCD00082767 |
Formula : | C7H5ClN2 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | YSBNBAYNISAUIT-UHFFFAOYSA-N |
M.W : | 152.58 | Pubchem ID : | 520400 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P305+P351+P338 | UN#: | |
Hazard Statements: | H302+H312+H332-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
72% | With triethylamine; In N,N-dimethyl-formamide; for 18.0h;Reflux; | General procedure: A mixture of 2-chloro-6-methylnicotinonitrile (II)(1.52 g, 0.01 mol) and corresponding sulfonamide derivatives (0.012 mol) in dry dimethylformamide(10 mL) containing 3 drops of trimethylamine was refluxed for 18 h then left to cool. The solid productformed upon pouring onto ice water was collected byfiltration and recrystallized from ethanol-dimethylformamide to give (III-XX), respectively. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
88% | With triethylamine; In N,N-dimethyl-formamide; for 18h;Reflux; | General procedure: A mixture of 2-chloro-6-methylnicotinonitrile (II)(1.52 g, 0.01 mol) and corresponding sulfonamide derivatives (0.012 mol) in dry dimethylformamide(10 mL) containing 3 drops of trimethylamine was refluxed for 18 h then left to cool. The solid productformed upon pouring onto ice water was collected byfiltration and recrystallized from ethanol-dimethylformamide to give (III-XX), respectively. |
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