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CAS No. : | 26750-81-2 | MDL No. : | MFCD00865165 |
Formula : | C13H17NO4 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | UMJHTFHIQDEGKB-UHFFFAOYSA-N |
M.W : | 251.28 | Pubchem ID : | 71916 |
Synonyms : |
|
Chemical Name : | 5-Allyl-2-hydroxy-N-(2-hydroxyethyl)-3-methoxybenzamide |
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
8.8 g | In toluene; for 12h;Reflux; Inert atmosphere; | Under a nitrogen atmosphere, 11.2 g of <strong>[85614-43-3]methyl 2-hydroxy-3-methoxy-5-allylbenzoate</strong> (5) and 80 ml of toluene were added to the reaction flask.After stirring uniformly, 12 ml of ethanolamine was added dropwise, and the mixture was heated under reflux for 12 hours.After completion of the reaction, the temperature was lowered, and the toluene phase was washed with 25 ml of 5% diluted hydrochloric acid, dried over anhydrous sodium sulfate and evaporated to dryness.The crude product was purified by recrystallization from 5 times benzene.The white powder alibendol 8.8 g was obtained in a purity of 98.6%. |