Purity | Size | Price | VIP Price | USA Stock *0-1 Day | Global Stock *5-7 Days | Quantity | ||||||
{[ item.p_purity ]} | {[ item.pr_size ]} | Inquiry |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,item.pr_rate,1,item.pr_is_large_size_no_price) ]} |
{[ getRatePrice(item.pr_usd, 1,1,item.pr_is_large_size_no_price) ]} | Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price) ]} {[ getRatePrice(item.pr_usd,1,item.mem_rate,item.pr_is_large_size_no_price) ]} | {[ item.pr_usastock ]} | in stock Inquiry - | {[ item.pr_chinastock ]} | {[ item.pr_remark ]} in stock Inquiry - | Login | Inquiry |
Please Login or Create an Account to: See VIP prices and availability
CAS No. : | 2243-81-4 | MDL No. : | MFCD00014314 |
Formula : | C11H9NO | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | RMHJJUOPOWPRBP-UHFFFAOYSA-N |
M.W : | 171.20 | Pubchem ID : | 75244 |
Synonyms : |
|
Chemical Name : | 1-Naphthamide |
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P301+P312-P302+P352-P304+P340-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
General synthetic procedure: Cyanoguanidine 2 (0.084 g, 1 mmol) is suspended in 2 mL of neat aromatic substrate (alternatively, the arene may be suspended in CH2Cl2) and freshly distilled triflic acid (0.5 mL, 6 mmol) is slowly added. The mixture is stirred at 60 °C for 2 h, after which 1 mL of cold water is added to the solution. The mixture is then stirred overnight. Product isolation is accomplished with basification of the mixture using 10 M NaOH and extraction of the mixture twice with chloroform. The organic extracts are washed with water, and then brine, and dried with anhydrous MgSO4. Crude products may be further purified by silica gel column chromatography (hexanes:ethyl acetate). |