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Chemical Structure| 2162-98-3 Chemical Structure| 2162-98-3
Chemical Structure| 2162-98-3

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CAS No.: 2162-98-3

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Product Details of 1,10-Dichlorodecane

CAS No. :2162-98-3
Formula : C10H20Cl2
M.W : 211.17
SMILES Code : ClCCCCCCCCCCCl
MDL No. :MFCD00000957
InChI Key :RBBNTRDPSVZESY-UHFFFAOYSA-N
Pubchem ID :75101

Safety of 1,10-Dichlorodecane

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H302-H315-H318-H410
Precautionary Statements:P280-P301+P312+P330-P305+P351+P338+P310
Class:9
UN#:3082
Packing Group:Ⅲ

Application In Synthesis of 1,10-Dichlorodecane

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2162-98-3 ]

[ 2162-98-3 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 4224-62-8 ]
  • [ 2162-98-3 ]
  • 2
  • [ 18528-78-4 ]
  • [ 2162-98-3 ]
  • N,N′-(decane-1,10-diyl)bis(9-amino-2,3-dihydro-1H-cyclopenta[b]quinolinium)dichloride [ No CAS ]
YieldReaction ConditionsOperation in experiment
4.5% In sulfolane; at 190 - 200℃; for 90.0h; A mixture of <strong>[18528-78-4]2,3-dihydro-1H-cyclopenta[b]quinolin-9-ylamine</strong> (0.45 g, 2.44 mmol), 1,10-dichlorodecane (0.25 g, 1.2mmol), and sulfolane (2 mL) was heated at 190-200 C for 90 h. The resulting mass was stirred with methanol and filtered. The filtrate was concentrated and chromatographedon an Al2O3 column using a gradient from 1 to 25% ofmethanol in methylene chloride. Fractions containing required product were pooled together and evaporated, andthe resulting off-white solid (31 mg, 4.5%) was further purified by crystallization from a methanol/acetone mixture [Mp 250-258 C (dec). 1H NMR (500 MHz, CDCl3) δ1.27-1.43 (m, 12 H), 1.67-1.76 (m, 4 H), 2.20-2.26 (m, 4H), 2.95 (t, 4 H, J = 7.5 Hz), 3.38 (t, 4 H, J = 7.5 Hz), 3.63(t, 4 H, J = 7.0 Hz), 4.46 (t, 4 H, J = 6.5 Hz),7.72 (t, 2 H, J = 7.0 Hz), 7.98 (t, 2 H, J = 7.5 Hz),8.15 (d, 2 H, J = 9.0 Hz), 8.54 (d with fine splitting, 2 H,J = 8.5 Hz), 8.92 (br s, 4 H, NH2).
In sulfolane; at 190 - 200℃; for 10.0h; General procedure: General methods for the synthesis of CABs are reported in Sharma et al. 2018 (Supra) and summarized in FIG. 5. Methods described in FIG. 5 are a) Amyl alcohol, reflux under N2, 12 h; b) No solvent, 180-195 C, 2 h; c) sulfolane, 190-200 C, 10 h. Three new CABs e.g. APDE-8, CODE-9 and CYDE-21 were successfully synthesized using the methods shown in FIG. 5.
 

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