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Ethanolamine is a viscous, hygroscopic amino alcohol with an ammoniacal odor. It is widely distributed in biological tissue and is a component of lecithin.
Synonyms: Monoethanolamine hydrochloride; Ethanolamine hydrochloride; 2-Aminoethanol hydrochloride
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Batch number can be found on the product's label following the word 'Batch'.
Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.
Search for reports by entering the product batch number.
Batch number can be found on the product's label following the word 'Batch'.
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Batch number can be found on the product's label following the word 'Batch'.
CAS No. : | 2002-24-6 |
Formula : | C2H8ClNO |
M.W : | 97.54 |
SMILES Code : | NCCO.[H]Cl |
Synonyms : |
Monoethanolamine hydrochloride; Ethanolamine hydrochloride; 2-Aminoethanol hydrochloride
|
MDL No. : | MFCD00012892 |
InChI Key : | PMUNIMVZCACZBB-UHFFFAOYSA-N |
Pubchem ID : | 74819 |
GHS Pictogram: |
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Signal Word: | Warning |
Hazard Statements: | H315-H319-H335 |
Precautionary Statements: | P261-P305+P351+P338 |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
98% | With thionyl chloride; In N-methyl-acetamide; water; benzene; | EXAMPLE 7 A mixture of 975 g. of <strong>[2002-24-6]monoethanolamine hydrochloride</strong>, 3.7 g. of dimethylformamide and 3500 g. of benzene was heated to 75 to 80C., and 1404 g. of thionylchloride were added dropwise thereto over 7 hours at the same temperature. After the addition was completed, the reaction solution was kept at the same temperature for further 1 hour and cooled to 30C., and then 2900 g. of water was added thereto. Then the solution was allowed to stand to separate into the benzene and aqueous layers. 4150 g. of the aqueous layer thus obtained contained 2-chloroethylamine hydrochloride which was produced in 98 % of yield, and 2.7 % by weight of free sulfur dioxide based on the aqueous layer. |
95% | With thionyl chloride; In toluene; at 75℃; for 3h; | Reagents and reaction conditions: SOCl2, Toluene, 75 Necked flask was added 15.0g of ethanolamine hydrochloride M-07 and toluene 15mL, stirring in an oil bath heated to 75 , the pressure-equalizing dropping funnel was slowly added dropwise 20.0g of thionyl chloride, the reaction ends after 3h. Cooling to room temperature, suction filtered, the filter cake was washed with a small amount of toluene and the toluene filtrate recovery next reuse. The filter cake was dried in vacuo to give a white solid 2-chloro-ethylamine hydrochloride 16.9g, that is, M-08, 95% yield. |