Alternatived Products of [ 1896-62-4 ]
Product Details of [ 1896-62-4 ]
| CAS No. : | 1896-62-4 |
MDL No. : | MFCD00008779 |
| Formula : |
C10H10O
|
Boiling Point : |
No data available |
| Linear Structure Formula : | C6H5CHCHC(O)CH3 |
InChI Key : | BWHOZHOGCMHOBV-BQYQJAHWSA-N |
| M.W : |
146.19
|
Pubchem ID : | 637759 |
| Synonyms : |
trans-Benzalacetone
|
Chemical Name : | (E)-4-Phenylbut-3-en-2-one |
Application In Synthesis of [ 1896-62-4 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Upstream synthesis route of [ 1896-62-4 ]
- Downstream synthetic route of [ 1896-62-4 ]
- 1
-
[ 4139-61-1 ]
-
[ 1896-62-4 ]
-
6-bromo-4-hydroxy-3-(3-oxo-1-phenylbutyl)chromen-2-one
[ No CAS ]
- 2
-
[ 391-12-8 ]
-
[ 1896-62-4 ]
-
[ 1373957-39-1 ]
-
[ 1373957-40-4 ]
| Yield | Reaction Conditions | Operation in experiment |
|
With QD-4; In tetrahydrofuran; at 20℃; for 48h; |
General procedure: In an ordinary vial equipped with a Teflon-coated stir bar, thiourea IV or V (0.04 mmol, 11.89 mg, 20 mol percent) was dissolved in 1.0 mL of THF. Then the corresponding isatins 1 (0.1 mmol, 1.0 equiv) was added, followed by the addition of alpha,beta-unsaturated ketones 2 (0.2 mmol, 2.0 equiv). The vial was capped with a rubber stopper and the mixture was stirred at room temperature for the time given in the tables. The crude mixture was then purified by flash column chromatography silica gel, using hexane/ethylacetate 2:1 as the eluent. Solvent was removed in vacuo to give the desired products. |
|
With 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1S)-(6-methoxyquinolin-4-yl)(5-vinylquinuclidin-2-yl)methyl)thiourea; In tetrahydrofuran; at 20℃; for 48h; |
General procedure: In an ordinary vial equipped with a Teflon-coated stir bar, thiourea IV or V (0.04 mmol, 11.89 mg, 20 mol percent) was dissolved in 1.0 mL of THF. Then the corresponding isatins 1 (0.1 mmol, 1.0 equiv) was added, followed by the addition of alpha,beta-unsaturated ketones 2 (0.2 mmol, 2.0 equiv). The vial was capped with a rubber stopper and the mixture was stirred at room temperature for the time given in the tables. The crude mixture was then purified by flash column chromatography silica gel, using hexane/ethylacetate 2:1 as the eluent. Solvent was removed in vacuo to give the desired products. |
- 3
-
[ 1896-62-4 ]
-
[ 3347-62-4 ]
- 4
-
[ 82771-60-6 ]
-
[ 1896-62-4 ]
-
(4R,11bS)-10-chloro-4-phenyl-1,3,4,6,7,11b-hexahydro-2H-pyrido[2,1-a]isoquinolin-2-one
[ No CAS ]
-
(4S,11bR)-10-chloro-4-phenyl-1,3,4,6,7,11b-hexahydro-2H-pyrido[2,1-a]isoquinolin-2-one
[ No CAS ]
-
10-chloro-4-phenyl-1,3,4,6,7,11b-hexahydro-2H-pyrido[2,1-a]isoquinolin-2-one
[ No CAS ]
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